1269508-31-7

Basic information

• Product Name: 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine
• Synonyms: 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine
• CAS NO: 1269508-31-7
• Molecular Formula: C27H26BN3O2
• Molecular Weight: 435.32524
• Mol File: 1269508-31-7.mol
• Article Data: 33

Chemical Properties

• Melting Point: 204 °C
• Boiling Point: 641.3±57.0 °C(Predicted)
• Appearance: /
• Density: 1.21±0.1 g/cm3(Predicted)
• PKA: 0.92±0.10(Predicted)
• CAS DataBase Reference: 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine(CAS DataBase Reference)
• NIST Chemistry Reference: 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine(1269508-31-7)
• EPA Substance Registry System: 2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine(1269508-31-7)

Safety Data

• Hazardous Substances Data: 1269508-31-7(Hazardous Substances Data)

Usage

Uses

2,4-Diphenyl-6-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,5-triazine can be used as an intermediate in organic synthesis, mainly used in laboratory research and development and chemical production processes.

Synthesis

15.0 g of 2-(3-Bromophenyl)-4,6-diphenyl-l,3,5- triazine (32.4 mmol), 12.3 g of bis(pinacolato)diboron (48.6 mmol), 529 mg of Pd(dppf)Cl2.CH2Cl2 (0.647 mmol), 9.53 g of potassium acetate (97.1 mmol) and 323 ml of dioxane were put into a 1-neck round flask and reacted under reflux at 90° C. for 12 hours. After completion of the reaction, the solvent was removed under reduced pressure. The produced solid was dissolved in dichloromethane and then filtered through a Celite filter and washed with dichloromethane. The solvent was removed under reduced pressure and the resultant compound was crystallized with methanol to obtain 16.0 g of solid compound (intermediate 6) (yield: 96.8%).

Upstream product

• 594823-67-3 (3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)bromobenzene) 
• 3842-55-5 2-chloro-4,6-diphenyl-1,3,5-triazine 
• 196212-27-8 4,4,5,5-tetramethyl-2-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,3,2-dioxaborolane 
• 89598-96-9 (3-bromophenyl)boronic acid 
• 108-36-1 1,3-dibromobenzene 
• 63503-60-6 3-chlorophenylboronic acid 
• 108-86-1 bromobenzene 
• 73183-34-3 bis(pinacol)diborane 
• 307929-32-4 3-chloro-(4,6-diphenyl-1,3,5-triazin-2-yl)benzene 
• 864377-31-1 2-(3-bromophenyl)-4,6-diphenyl-[1,3,5]triazine 

Downstream Products

• 1443049-83-9 2-(3'-chloro-[1,1'-biphenyl]-3-yl)-4,6-diphenyl-1,3,5-triazine 

Relevant articles and documents

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