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13595-25-0

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13595-25-0 Usage

General Description

Bisphenol M is a bisphenol analog, used in a variety of industrial applications, such as the synthesis of polycarbonate and epoxy resins. It is also used in electronics, toys, food containers, bottles, papers, medical equipment, etc.

Flammability and Explosibility

Nonflammable

Check Digit Verification of cas no

The CAS Registry Mumber 13595-25-0 includes 8 digits separated into 3 groups by hyphens. The first part of the number,starting from the left, has 5 digits, 1,3,5,9 and 5 respectively; the second part has 2 digits, 2 and 5 respectively.
Calculate Digit Verification of CAS Registry Number 13595-25:
(7*1)+(6*3)+(5*5)+(4*9)+(3*5)+(2*2)+(1*5)=110
110 % 10 = 0
So 13595-25-0 is a valid CAS Registry Number.

13595-25-0 Well-known Company Product Price

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  • Sigma-Aldrich

  • (23454)  Bisphenol?M  analytical standard

  • 13595-25-0

  • 23454-100MG

  • 458.64CNY

  • Detail
  • Aldrich

  • (450464)  4,4′-(1,3-Phenylenediisopropylidene)bisphenol  99%

  • 13595-25-0

  • 450464-100G

  • 1,265.94CNY

  • Detail

13595-25-0SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 1,3-Bis[2-(4-hydroxyphenyl)-2-propyl]benzene

1.2 Other means of identification

Product number -
Other names 4-[2-[3-[2-(4-hydroxyphenyl)propan-2-yl]phenyl]propan-2-yl]phenol

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:13595-25-0 SDS

13595-25-0Synthetic route

1,3-bis(1',1'-dimethylhydroxymethyl)benzene
1999-85-5

1,3-bis(1',1'-dimethylhydroxymethyl)benzene

phenol
108-95-2

phenol

bisphenol M
13595-25-0

bisphenol M

bisphenol M
13595-25-0

bisphenol M

4-picolylchloride hydrochloride
1822-51-1

4-picolylchloride hydrochloride

C36H36N2O2
1020725-78-3

C36H36N2O2

Conditions
ConditionsYield
With sodium hydroxide; tetra(n-butyl)ammonium hydroxide In benzene at 80℃; for 48h;98%
2-chloropyrazin
14508-49-7

2-chloropyrazin

bisphenol M
13595-25-0

bisphenol M

1,3-di(2-(4-(2-pyrazinyloxy)phenyl)prop-2-yl)benzene
1020725-53-4

1,3-di(2-(4-(2-pyrazinyloxy)phenyl)prop-2-yl)benzene

Conditions
ConditionsYield
Stage #1: bisphenol M With potassium carbonate In sulfolane; toluene at 20℃; for 0.75h;
Stage #2: 2-chloropyrazin at 80℃; for 48h; Further stages.;
94%
bromocyane
506-68-3

bromocyane

bisphenol M
13595-25-0

bisphenol M

bisphenol M cyanate

bisphenol M cyanate

Conditions
ConditionsYield
With triethylamine; isopropyl alcohol In acetone at -15 - -10℃; for 2.5h;93%
4-Nitrophthalonitrile
31643-49-9

4-Nitrophthalonitrile

bisphenol M
13595-25-0

bisphenol M

C40H30N4O2

C40H30N4O2

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide at 20℃; for 48h; Inert atmosphere;91.3%
bisphenol M
13595-25-0

bisphenol M

3-chloromethylpyridinium chloride
6959-48-4

3-chloromethylpyridinium chloride

1,3-di(2-(4-(3-pyridylmethoxy)phenyl)prop-2-yl)benzene
1020725-73-8

1,3-di(2-(4-(3-pyridylmethoxy)phenyl)prop-2-yl)benzene

Conditions
ConditionsYield
With sodium hydroxide; tetra(n-butyl)ammonium hydroxide In benzene at 80℃; for 48h;90.4%
bisphenol M
13595-25-0

bisphenol M

2-chloromethylpyridine hydrochloride
6959-47-3

2-chloromethylpyridine hydrochloride

C36H36N2O2
1020725-68-1

C36H36N2O2

Conditions
ConditionsYield
With sodium hydroxide; tetra(n-butyl)ammonium hydroxide In benzene at 80℃; for 48h;84%
bisphenol M
13595-25-0

bisphenol M

A

C72H72O6P2

C72H72O6P2

B

C72H72O6P2

C72H72O6P2

Conditions
ConditionsYield
With TEA; phosphorus trichloride In toluene at 25℃; for 24h;A n/a
B 18%
bisphenol M
13595-25-0

bisphenol M

A

C72H72O6P2

C72H72O6P2

B

C72H72O6P2

C72H72O6P2

Conditions
ConditionsYield
With TEA; phosphorus trichloride In toluene at 25℃; for 24h;A n/a
B 18%
bisphenol M
13595-25-0

bisphenol M

A

C72H72O8P2

C72H72O8P2

B

C72H72O8P2

C72H72O8P2

Conditions
ConditionsYield
Stage #1: bisphenol M With TEA; phosphorus trichloride In toluene at 25℃; for 24h;
Stage #2: With Cumene hydroperoxide In toluene at 20℃; for 1h;
A n/a
B 1.37 g
bisphenol M
13595-25-0

bisphenol M

4-chlorobenzonitrile
100-00-5

4-chlorobenzonitrile

1,3-bis[4-(4-nitrophenoxy)-α,α-dimethylbenzyl]benzene
135672-39-8

1,3-bis[4-(4-nitrophenoxy)-α,α-dimethylbenzyl]benzene

Conditions
ConditionsYield
With potassium carbonate In water; N,N-dimethyl-formamide; toluene
meta-dinitrobenzene
99-65-0

meta-dinitrobenzene

bisphenol M
13595-25-0

bisphenol M

1,3-bis[4-(3-nitrophenoxy)-α,α-dimethylbenzyl]benzene
135654-83-0

1,3-bis[4-(3-nitrophenoxy)-α,α-dimethylbenzyl]benzene

Conditions
ConditionsYield
With potassium carbonate In water; N,N-dimethyl-formamide; toluene
formaldehyd
50-00-0

formaldehyd

bisphenol M
13595-25-0

bisphenol M

4,4'-[1,3-phenylenebis(1-methylethylidene)]bis(3,5-dihydroxymethylphenol)

4,4'-[1,3-phenylenebis(1-methylethylidene)]bis(3,5-dihydroxymethylphenol)

Conditions
ConditionsYield
Stage #1: bisphenol M With sodium hydroxide In methanol; water at 20℃; for 0.166667h;
Stage #2: formaldehyd In water at 30℃; for 9h;
bisphenol M
13595-25-0

bisphenol M

3-(4-(2-(3-(2-(4-(3-chloro-2-hydroxypropoxy)phenyl)propan-2-yl)phenyl)propan-2-yl)phenoxy)propane-1,2-diol
1403962-95-7

3-(4-(2-(3-(2-(4-(3-chloro-2-hydroxypropoxy)phenyl)propan-2-yl)phenyl)propan-2-yl)phenoxy)propane-1,2-diol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C / Inert atmosphere
1.2: 40 h / 70 - 80 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C / Inert atmosphere
2.2: 22 h / 20 °C / Inert atmosphere
3.1: cerium(III) chloride heptahydrate / acetonitrile / 22 h / Reflux
View Scheme
5-chloromethyl-2,2-dimethyl-1,3-dioxolane
4362-40-7

5-chloromethyl-2,2-dimethyl-1,3-dioxolane

bisphenol M
13595-25-0

bisphenol M

2,2-dimethyl-4-((4-(2-(3-(2-(4-(oxiran-2-ylmethoxy)phenyl)propan-2-yl)phenyl)propan-2-yl)phenoxy)methyl)-1,3-dioxolane
1403962-94-6

2,2-dimethyl-4-((4-(2-(3-(2-(4-(oxiran-2-ylmethoxy)phenyl)propan-2-yl)phenyl)propan-2-yl)phenoxy)methyl)-1,3-dioxolane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C / Inert atmosphere
1.2: 40 h / 70 - 80 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 20 °C / Inert atmosphere
2.2: 22 h / 20 °C / Inert atmosphere
View Scheme
bisphenol M
13595-25-0

bisphenol M

p-acetylaminobenzenesulfonyl chloride
121-60-8

p-acetylaminobenzenesulfonyl chloride

C40H40N2O8S2

C40H40N2O8S2

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 30 - 40℃; for 3h; Inert atmosphere;
bisphenol M
13595-25-0

bisphenol M

3-fluoro-6-nitrotoluene
446-33-3

3-fluoro-6-nitrotoluene

1,3-bis{2-[4-(3-methyl-4-nitrophenoxy)phenyl]-2-propyl}benzene

1,3-bis{2-[4-(3-methyl-4-nitrophenoxy)phenyl]-2-propyl}benzene

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 120℃; for 9h;6.0 g
bisphenol M
13595-25-0

bisphenol M

3-fluoro-6-nitrotoluene
446-33-3

3-fluoro-6-nitrotoluene

1,3-bis{2-[4-(4-amino-3-methylphenoxy)phenyl]-2-propyl}benzene

1,3-bis{2-[4-(4-amino-3-methylphenoxy)phenyl]-2-propyl}benzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 9 h / 120 °C
2: 5%-palladium/activated carbon; 2-methoxy-ethanol; hydrogen / 90 °C / 6000.6 Torr / Autoclave
View Scheme

13595-25-0Relevant articles and documents

MEDICAL DEVICE USING SULFONATED NEUTRALIZED POLYMERS WITH REDUCED ADHESION OF BIOLOGICAL FLUIDS

-

, (2010/05/13)

A medical article having neutralized sulfonic acid groups on its surface, is disclosed. The article has reduced interaction with biological fluids such as insulin, human growth hormone and human serum albumin.

Production process of bisphenol compounds

-

, (2008/06/13)

A process for the production of a bisphenol compound comprising: a step for reacting a phenolic compound (a) with at least one compound (b) selected from the group consisting of dialkenylbenzene compounds, bis(hydroxyalkyl)benzene compounds and (hydroxyalkyl)-alkenylbenzene compounds or at least one compound (c) selected from the group consisting of monoalkenylphenolic compounds and mono(hydroxyalkyl)phenolic compounds in the presence of an acidic catalyst to obtain a reaction mixture containing said bisphenol compound, a step for neutralizing the reaction mixture with an anion exchange resin, a step for removing a remaining phenolic compound from the reaction mixture to concentrate the neutralized reaction mixture, and a step for isolating the bisphenol compound from the resulting concentrated mixture. This process enables to produce a bisphenol compound, which is useful for preparing raw materials of thermoplastic polymers, surface-active agents and stabilizers.

Phenolic compounds

-

, (2008/06/13)

A phenolic compound having formula (I): STR1 wherein X represents a chlorine atom or a methyl group, and a recording material comprising a coloress or light-colored leuco dye and the above phenolic compound serving as a color developer for the leuco dye are disclosed.

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