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13963-57-0 Usage

Health Hazard

Exposures to aluminium (III) acetylacetonate cause adverse health effects. Exposures by inhalation, ingestion, and through skin contact are harmful. It causes irritation effects to the eyes, skin, and respiratory tract. Aluminium (III) acetylacetonate may release 2,4-pentanedione, which is a suspected teratogen and causes neurological health effects and harm to the unborn child. However, toxicology is not fully investigated.

Purification Methods

Recrystallise it several times from *benzene or aqueous MeOH, 216 and 286mn. max [Charles & Pawlikowski J Phys Chem 62 440 1958.] It can be purified by sublimation and has the following solubilities in g percent: *C6H6 35.9 (20o), 47.6 (40o), toluene 15.9 (20o), 22.0 (40o) and acetylacetone 6.6 (20o), 10.4 (40o). [Fernelius & Bryant Inorg Synth V 105 1957, Beilstein 1 IV 3668.]

Uses

Aluminum acetylacetonate is an important organic intermediate (building block) to synthetize substituted acetylacetonate products.

Chemical Properties

Aluminium (III) acetylacetonate is a white to yellow powder or crystals in appearance. It is stable and incompatible with strong oxidizing agents.

Uses

Deposition of aluminum, catalyst.
InChI:InChI=1/3C5H8O2.Al/c3*1-4(6)3-5(2)7;/h3*3,6H,1-2H3;/q;;;+3/p-3/b3*4-3-;

13963-57-0 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (12542)  Aluminum 2,4-pentanedionate    13963-57-0 100g 355.0CNY Detail
Alfa Aesar (12542)  Aluminum 2,4-pentanedionate    13963-57-0 500g 1164.0CNY Detail
Alfa Aesar (44538)  Aluminum 2,4-pentanedionate, 99.995+% (metals basis)    13963-57-0 5g 625.0CNY Detail
Alfa Aesar (44538)  Aluminum 2,4-pentanedionate, 99.995+% (metals basis)    13963-57-0 25g 2408.0CNY Detail
Alfa Aesar (44538)  Aluminum 2,4-pentanedionate, 99.995+% (metals basis)    13963-57-0 100g 7594.0CNY Detail
Aldrich (674753)  Aluminumacetylacetonate  purified by sublimation, 99.999% trace metals basis 13963-57-0 674753-5G 525.33CNY Detail
Aldrich (674753)  Aluminumacetylacetonate  purified by sublimation, 99.999% trace metals basis 13963-57-0 674753-25G 1,818.18CNY Detail
Aldrich (208248)  Aluminumacetylacetonate  ReagentPlus®, 99% 13963-57-0 208248-100G 402.48CNY Detail
Aldrich (208248)  Aluminumacetylacetonate  ReagentPlus®, 99% 13963-57-0 208248-500G 1,404.00CNY Detail

13963-57-0SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 12, 2017

Revision Date: Aug 12, 2017

1.Identification

1.1 GHS Product identifier

Product name Aluminum acetylacetonate

1.2 Other means of identification

Product number -
Other names ALUMINUM(III) AA

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:13963-57-0 SDS

13963-57-0Synthetic route

aluminum hydroxide

aluminum hydroxide

acetylacetone
123-54-6

acetylacetone

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

Conditions
ConditionsYield
at 0 - 50℃; for 0.75h;91%
acetylacetone
123-54-6

acetylacetone

AlCl3

AlCl3

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

Conditions
ConditionsYield
With chloroform
With ammonia; water
acetylacetone
123-54-6

acetylacetone

Al(OH)3

Al(OH)3

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

acetyl chloride
75-36-5

acetyl chloride

AlCl3

AlCl3

A

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

B

acetylacetone
123-54-6

acetylacetone

copper bis(tetraisopropoxyaluminate)
70504-66-4, 45188-39-4

copper bis(tetraisopropoxyaluminate)

acetylacetone
123-54-6

acetylacetone

A

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

B

copper(II) acetylacetonate
13395-16-9

copper(II) acetylacetonate

Conditions
ConditionsYield
In benzene byproducts: i-propanol; the i-propoxy-complex and acetylacetone (1:8 molar ratio) were refluxedin benzene for 10 h (isopropanol was removed azeotropically out between72-80°C along with benzene); removing the solvent; elem. anal.;
aluminium trichloride
7446-70-0

aluminium trichloride

acetylacetone
123-54-6

acetylacetone

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

Conditions
ConditionsYield
In water in acidic medium;
tris(o-chlorophenoxo)aluminium(III)

tris(o-chlorophenoxo)aluminium(III)

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

Conditions
ConditionsYield
With acetylacetone In benzene stirring Al complex and diketone (molar ratio 1/6, slight excess) with stirring, 6h; aaddn. of petroleum ether; pptn.; recrystn. (benzene/acetone); elem. anal.;
lithium aluminium tetrahydride
16853-85-3

lithium aluminium tetrahydride

nickel(II) acetylacetonate
3264-82-2

nickel(II) acetylacetonate

A

aluminium hydride

aluminium hydride

B

nickel
7440-02-0

nickel

C

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

D

lithium pentane-2,4-dionate
18115-70-3

lithium pentane-2,4-dionate

Conditions
ConditionsYield
In tetrahydrofuran; benzene byproducts: H2; various product ratios at various reactant ratios; not isolated, detected by GLC, UV, IR;
aluminium(III) sulfate hexadecahydrate

aluminium(III) sulfate hexadecahydrate

acetylacetone
123-54-6

acetylacetone

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

Conditions
ConditionsYield
Stage #1: acetylacetone With ammonia In water
Stage #2: aluminium(III) sulfate hexadecahydrate In water
C65H75N7O20

C65H75N7O20

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

2,3,9,10,16,17,23,24-tetra(15-crown-5)phthalocyaninatoaluminum(III) hydroxide

2,3,9,10,16,17,23,24-tetra(15-crown-5)phthalocyaninatoaluminum(III) hydroxide

Conditions
ConditionsYield
With 1,2,3-trichlorobenzene; phenol In octanol93%
aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

tetra(15-crown-5)ed phthalocyanine
110682-72-9

tetra(15-crown-5)ed phthalocyanine

2,3,9,10,16,17,23,24-tetra(15-crown-5)phthalocyaninatoaluminum(III) hydroxide

2,3,9,10,16,17,23,24-tetra(15-crown-5)phthalocyaninatoaluminum(III) hydroxide

Conditions
ConditionsYield
With phenol In octanol; chloroform for 2h; Inert atmosphere; Reflux;93%
methanol
67-56-1

methanol

C60H45BN4O6

C60H45BN4O6

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

C62H50AlBN4O8

C62H50AlBN4O8

Conditions
ConditionsYield
In chloroform for 21h; Reflux;29%
aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

A

methylammonium carbonate
15719-64-9, 15719-76-3, 97762-63-5

methylammonium carbonate

B

acetone
67-64-1

acetone

Conditions
ConditionsYield
at 200 - 400℃; Pyrolysis;
fumaryl-bis-N-phenyl hydroxamic acid
87839-04-1

fumaryl-bis-N-phenyl hydroxamic acid

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

Al(3+)*CH3COCHCOCH3(1-)*(CHCONOC6H5)2(2-)*3H2O=(Al(CH3COCHCOCH3)(CHCONOC6H5)2*3H2O)

Al(3+)*CH3COCHCOCH3(1-)*(CHCONOC6H5)2(2-)*3H2O=(Al(CH3COCHCOCH3)(CHCONOC6H5)2*3H2O)

Conditions
ConditionsYield
With H2O In ethanol; N,N-dimethyl-formamide mixt. of ligand and metal acetylacetonate in DMF/ethanol (1:4) is heated on a water-bath; washing with DMF/ethanol; elem. anal.;
aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

fumaryl-bis-N-m-tolylhydroxamic acid

fumaryl-bis-N-m-tolylhydroxamic acid

Al(3+)*CH3COCHCOCH3(1-)*(CHCONOC6H4CH3)2(2-)*2H2O=(Al(CH3COCHCOCH3)(CHCONOC6H4CH3)2*2H2O)

Al(3+)*CH3COCHCOCH3(1-)*(CHCONOC6H4CH3)2(2-)*2H2O=(Al(CH3COCHCOCH3)(CHCONOC6H4CH3)2*2H2O)

Conditions
ConditionsYield
With H2O In ethanol; N,N-dimethyl-formamide mixt. of ligand and metal acetylacetonate in DMF/ethanol (1:4) is heated on a water-bath; washing with DMF/ethanol; elem. anal.;
phosphoric acid
86119-84-8, 7664-38-2

phosphoric acid

vanadia

vanadia

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

VO(2+)*HPO4(2-)*0.5H2O=VOHPO4*0.5H2O#dotAl

VO(2+)*HPO4(2-)*0.5H2O=VOHPO4*0.5H2O#dotAl

Conditions
ConditionsYield
With 2-methyl-propan-1-ol; water In further solvent(s) V2O5 and aluminium acetylacetonate refluxed with H3PO4 in isobutanol for16 h, filtered, washed (isobutanol/ethanol), refluxed with water for 3 h; filtration, drying in air, XRD;
yttrium(lll) nitrate hexahydrate

yttrium(lll) nitrate hexahydrate

erbium(III) nitrate pentahydrate

erbium(III) nitrate pentahydrate

Triisopropyl borate
5419-55-6

Triisopropyl borate

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

yttrium erbium aluminum borate

yttrium erbium aluminum borate

Conditions
ConditionsYield
In ethanol; acetic acid; propionic acid sol-gel method; powders were mixed under N2, solvents were added, after complete dissolution at 80°C for 2-6 h water was added for hydrolysis at 80°C, 1 h, (0.9 Y:0.1 Er:3 Al:4 B:5H2O; then solvents were slow evapd. at 80°C for 14 d; resulting gels were heated at different temp. to eliminate the organic comp. and crystallize composition under O2-rich atm.; XRD;
zinc(II) propionate
557-28-8

zinc(II) propionate

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

(ZnO)0.30(Al2O3)070

(ZnO)0.30(Al2O3)070

Conditions
ConditionsYield
In ethanol mixing solns. of stoich. amounts of alumatrane and zinc acetate, addn. of ethanol, stirring at room temp., aerosolizing with O2, igniting at 1500-200°C; powder XRD;
zinc(II) propionate
557-28-8

zinc(II) propionate

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

A

zinc aluminate

zinc aluminate

B

(ZnO)0.80(Al2O3)020

(ZnO)0.80(Al2O3)020

Conditions
ConditionsYield
In ethanol mixing solns. of stoich. amounts of alumatrane and zinc acetate, addn. of ethanol, stirring at room temp., aerosolizing with O2, igniting at 1500-200°C; powder XRD;
zinc(II) propionate
557-28-8

zinc(II) propionate

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

(ZnO)0.95(Al2O3)005

(ZnO)0.95(Al2O3)005

Conditions
ConditionsYield
In ethanol mixing solns. of stoich. amounts of alumatrane and zinc acetate, addn. of ethanol, stirring at room temp., aerosolizing with O2, igniting at 1500-200°C; powder XRD;
zinc(II) propionate
557-28-8

zinc(II) propionate

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

(ZnO)0.99(Al2O3)001

(ZnO)0.99(Al2O3)001

Conditions
ConditionsYield
In ethanol mixing solns. of stoich. amounts alumatrane and zinc acetate, addn. of ethanol, stirring at room temp., aerosolizing with O2, igniting at 1500-200°C; powder XRD;
zinc(II) propionate
557-28-8

zinc(II) propionate

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

A

zinc aluminate

zinc aluminate

alumina

alumina

Conditions
ConditionsYield
In ethanol mixing solns. of alumatrane and zinc acetate in 9:1 molar ratio, addn. of ethanol, stirring at room temp., aerosolizing with O2, igniting at 1500-200°C; quenching to room temp., powder XRD;
zinc(II) propionate
557-28-8

zinc(II) propionate

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

zinc aluminate

zinc aluminate

Conditions
ConditionsYield
In ethanol mixing solns. of alumatrane and zinc acetate in 1:1 molar ratio, addn. of ethanol, stirring at room temp., aerosolizing with O2, igniting at 1500-200°C; quenching to room temp., powder XRD;
aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

cobalt(II) aceylacetonate

cobalt(II) aceylacetonate

iron(III) acetylacetonate

iron(III) acetylacetonate

Co1.2Fe1.3Al1.5

Co1.2Fe1.3Al1.5

Conditions
ConditionsYield
Stage #1: aluminium acetylacetonate; cobalt(II) aceylacetonate; iron(III) acetylacetonate With hexadecane-1,2-diol; (Z)-9-octadecen-1-amine; cis-Octadecenoic acid at 100℃; Schlenk technique; Reflux;
Stage #2: at 300 - 500℃;
aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

cobalt(II) aceylacetonate

cobalt(II) aceylacetonate

iron(III) acetylacetonate

iron(III) acetylacetonate

Co1.6Fe1.8Al0.6

Co1.6Fe1.8Al0.6

Conditions
ConditionsYield
Stage #1: aluminium acetylacetonate; cobalt(II) aceylacetonate; iron(III) acetylacetonate With hexadecane-1,2-diol; (Z)-9-octadecen-1-amine; cis-Octadecenoic acid at 100℃; Schlenk technique; Reflux;
Stage #2: at 300 - 700℃;
aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

cobalt(II) aceylacetonate

cobalt(II) aceylacetonate

iron(III) acetylacetonate

iron(III) acetylacetonate

Co1.4Fe1.3Al1.4

Co1.4Fe1.3Al1.4

Conditions
ConditionsYield
Stage #1: aluminium acetylacetonate; cobalt(II) aceylacetonate; iron(III) acetylacetonate With hexadecane-1,2-diol; (Z)-9-octadecen-1-amine; cis-Octadecenoic acid at 100℃; Schlenk technique; Reflux;
Stage #2: at 300 - 700℃;
iron(III)-acetylacetonate
14024-18-1

iron(III)-acetylacetonate

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

Fe2850Al0150O4

Fe2850Al0150O4

Conditions
ConditionsYield
In benzyl alcohol at 199.84℃; for 48h; Autoclave;
iron(III)-acetylacetonate
14024-18-1

iron(III)-acetylacetonate

aluminium acetylacetonate
13963-57-0

aluminium acetylacetonate

Al0.6Fe2.4O4

Al0.6Fe2.4O4

Conditions
ConditionsYield
In benzyl alcohol at 199.84℃; for 48h; Autoclave;
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