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high purity 1609373-99-0 2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine
Cas No: 1609373-99-0
USD $ 1.9-2.5 / Kilogram 1 Kilogram 999999 Kilogram/Year Hangzhou Dingyan Chem Co., Ltd Contact Supplier
Factory Price OLED 99% 1609373-99-0 2-methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine Manufacturer
Cas No: 1609373-99-0
USD $ 0.1-0.1 / Gram 1 Gram 100 Metric Ton/Year Xi'an Xszo Chem Co., Ltd. Contact Supplier
2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine 1609373-99-0
Cas No: 1609373-99-0
No Data 1 Metric Ton 100 Metric Ton/Day Henan Tianfu Chemical Co., Ltd. Contact Supplier
BLOOM TECH Advanced API/Technology support 2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine CAS 1609373-99-0
Cas No: 1609373-99-0
No Data 1 Gram 3 Metric Ton/Month Shaanxi BLOOM TECH Co.,Ltd Contact Supplier
2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine
Cas No: 1609373-99-0
No Data 1 Gram 1000 Kilogram/Day CHANGCHUN WEIERSI IMPORT AND EXPORT TRADE CO.,LTD Contact Supplier
1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
Cas No: 1609373-99-0
No Data No Data 10000 Metric Ton/Month Henan Wentao Chemical Product Co., Ltd. Contact Supplier
2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine/ LIDE PHARMA- Factory supply / Best price
Cas No: 1609373-99-0
No Data No Data 1 LIDE PHARMACEUTICALS LIMITED Contact Supplier
2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine
Cas No: 1609373-99-0
No Data 10 Gram 10000 Metric Ton/Month Changchun JuShengyuan Import and Export Trading Co.,Ltd Contact Supplier
Best facotry !!CAS 1609373-99-0 2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine CAS NO.1609373-99-0
Cas No: 1609373-99-0
No Data 10 Gram 500 Kilogram/Month Changchun Artel lmport and Export trade company Contact Supplier
2-Methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine 1609373-99-0
Cas No: 1609373-99-0
USD $ 1.0-9999.0 / Kilogram 1 Kilogram 1 Metric Ton/Week Changzhou Pesan Chemical Co.,Ltd Contact Supplier

1609373-99-0 Usage

1609373-99-0Synthetic route

2-bromo-pyridine
109-04-6

2-bromo-pyridine

2-methyl-8-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzofuro[2,3-b]pyridine
1609374-04-0

2-methyl-8-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzofuro[2,3-b]pyridine

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Stage #1: 2-bromo-pyridine; 2-methyl-8-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzofuro[2,3-b]pyridine With potassium carbonate In tetrahydrofuran for 0.5h; Inert atmosphere;
Stage #2: With tetrakis(triphenylphosphine) palladium(0) at 80℃; for 12h;
80%
2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate
1609373-98-9

2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

pyridin-2-ylzinc(II) bromide

pyridin-2-ylzinc(II) bromide

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); XPhos In tetrahydrofuran at 60 - 65℃; for 12h;65%
(2,3-dimethoxyphenyl)boronic acid
40972-86-9

(2,3-dimethoxyphenyl)boronic acid

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 5 h / Reflux
2: acetic acid; tert.-butylnitrite / tetrahydrofuran / 2 h / 0 °C
3: pyridine hydrochloride / 15 h / 200 °C
4: pyridine / dichloromethane / 0 °C
5: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
2-amino-3-bromo-6-methyl-pyridine
126325-46-0

2-amino-3-bromo-6-methyl-pyridine

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane; water / 5 h / Reflux
2: acetic acid; tert.-butylnitrite / tetrahydrofuran / 2 h / 0 °C
3: pyridine hydrochloride / 15 h / 200 °C
4: pyridine / dichloromethane / 0 °C
5: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
3-(2,3-dimethoxyphenyl)-6-methylpyridin-2-amine
1609373-95-6

3-(2,3-dimethoxyphenyl)-6-methylpyridin-2-amine

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: acetic acid; tert.-butylnitrite / tetrahydrofuran / 2 h / 0 °C
2: pyridine hydrochloride / 15 h / 200 °C
3: pyridine / dichloromethane / 0 °C
4: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
8-methoxy-2-methylbenzofuro[2,3-b]pyridine
1609373-96-7

8-methoxy-2-methylbenzofuro[2,3-b]pyridine

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: pyridine hydrochloride / 15 h / 200 °C
2: pyridine / dichloromethane / 0 °C
3: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
Multi-step reaction with 3 steps
1: pyridine hydrochloride / 200 °C
2: dichloromethane / 0 - 20 °C
3: magnesium / tetrahydrofuran / 35 - 45 °C
View Scheme
2-methylbenzofuro[2,3-b]pyridine-8-ol
1609373-97-8

2-methylbenzofuro[2,3-b]pyridine-8-ol

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine / dichloromethane / 0 °C
2: tris-(dibenzylideneacetone)dipalladium(0); XPhos / tetrahydrofuran / 12 h / 60 - 65 °C
View Scheme
2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate
1609373-98-9

2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene / 1,4-dioxane / 80 °C
2.1: potassium carbonate / tetrahydrofuran / 0.5 h / Inert atmosphere
2.2: 12 h / 80 °C
View Scheme
2-bromo-pyridine
109-04-6

2-bromo-pyridine

2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate
1609373-98-9

2-methylbenzofuran[2,3-b]pyridin-8-yl-trifluoromethanesulfonate

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
With magnesium In tetrahydrofuran at 35 - 45℃;
2-Amino-6-methylpyridine
1824-81-3

2-Amino-6-methylpyridine

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: N-chloro-succinimide; bromine / tetrahydrofuran / 25 - 30 °C
2: toluene; ethanol; water / Reflux
3: acetic acid; tert.-butylnitrite / tetrahydrofuran / -20 °C
4: hydrogen; sodium carbonate; palladium on activated charcoal / tetrahydrofuran / 20 - 60 °C
5: pyridine hydrochloride / 200 °C
6: dichloromethane / 0 - 20 °C
7: magnesium / tetrahydrofuran / 35 - 45 °C
View Scheme
3-bromo-5-chloro-6-methylpyridin-2-amine

3-bromo-5-chloro-6-methylpyridin-2-amine

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: toluene; ethanol; water / Reflux
2: acetic acid; tert.-butylnitrite / tetrahydrofuran / -20 °C
3: hydrogen; sodium carbonate; palladium on activated charcoal / tetrahydrofuran / 20 - 60 °C
4: pyridine hydrochloride / 200 °C
5: dichloromethane / 0 - 20 °C
6: magnesium / tetrahydrofuran / 35 - 45 °C
View Scheme
C14H15ClN2O2

C14H15ClN2O2

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: acetic acid; tert.-butylnitrite / tetrahydrofuran / -20 °C
2: hydrogen; sodium carbonate; palladium on activated charcoal / tetrahydrofuran / 20 - 60 °C
3: pyridine hydrochloride / 200 °C
4: dichloromethane / 0 - 20 °C
5: magnesium / tetrahydrofuran / 35 - 45 °C
View Scheme
C13H10ClNO2

C13H10ClNO2

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: hydrogen; sodium carbonate; palladium on activated charcoal / tetrahydrofuran / 20 - 60 °C
2: pyridine hydrochloride / 200 °C
3: dichloromethane / 0 - 20 °C
4: magnesium / tetrahydrofuran / 35 - 45 °C
View Scheme
1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

2-d3-methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine
1609374-00-6

2-d3-methyl-8-(pyridin-2-yl)benzofuro[2,3-b]pyridine

Conditions
ConditionsYield
With sodium ethanolate In ethyl [2]alcohol for 72h; Reflux;80%
With dimethylsulfoxide-d6; sodium t-butanolate at 80℃; for 12h;80%
1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

C28H40IrN2O2(1+)*CF3O3S(1-)

C28H40IrN2O2(1+)*CF3O3S(1-)

C43H43IrN4O

C43H43IrN4O

Conditions
ConditionsYield
In 2-ethoxy-ethanol; N,N-dimethyl-formamide at 130℃; for 18h;61%
1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

C26H36IrN2O2(1+)*CF3O3S(1-)

C26H36IrN2O2(1+)*CF3O3S(1-)

C41H39IrN4O

C41H39IrN4O

Conditions
ConditionsYield
In 2-ethoxy-ethanol; N,N-dimethyl-formamide at 130℃; for 18h;60%
1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

C24H32IrN2O2(1+)*CF3O3S(1-)

C24H32IrN2O2(1+)*CF3O3S(1-)

C39H35IrN4O

C39H35IrN4O

Conditions
ConditionsYield
In 2-ethoxy-ethanol; N,N-dimethyl-formamide at 130℃; for 18h;58%
1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

C24H26IrN2O2(1+)*CF3O3S(1-)
1215692-14-0, 1532554-40-7

C24H26IrN2O2(1+)*CF3O3S(1-)

C39H30IrN4O
1609368-30-0

C39H30IrN4O

Conditions
ConditionsYield
In ethanol for 20h; Reflux;46%
1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

C39H27(2)H3IrN4O
1609368-31-1

C39H27(2)H3IrN4O

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium ethanolate / ethyl [2]alcohol / 72 h / Reflux
2: 2-ethoxy-ethanol; N,N-dimethyl-formamide / 18 h / 130 °C
View Scheme
1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

C41H25(2)H9IrN4O
1609368-32-2

C41H25(2)H9IrN4O

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium ethanolate / ethyl [2]alcohol / 72 h / Reflux
2: 2-ethoxy-ethanol; N,N-dimethyl-formamide / 18 h / 130 °C / Inert atmosphere
View Scheme
1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

C41H30(2)H9IrN4O

C41H30(2)H9IrN4O

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium t-butanolate; dimethylsulfoxide-d6 / 12 h / 80 °C
2: 2-ethoxy-ethanol; N,N-dimethyl-formamide / 18 h / 130 °C
View Scheme
1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

C43H28(2)H15IrN4O

C43H28(2)H15IrN4O

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium t-butanolate; dimethylsulfoxide-d6 / 12 h / 80 °C
2: 2-ethoxy-ethanol; N,N-dimethyl-formamide / 18 h / 130 °C
View Scheme
iridium(III) chloride monohydrate

iridium(III) chloride monohydrate

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine
1609373-99-0

1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine

(1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine)4Ir2Cl2

(1,2-methyl-8-(2-pyridine)benzofuran[2,3-B]pyridine)4Ir2Cl2

Conditions
ConditionsYield
In 2-ethoxy-ethanol; water
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