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16227-10-4

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4-Butyl-4H-1,2,4-triazole Manufacturer/High quality/Best price/In stock
Cas No: 16227-10-4
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
6-quinolin-1-iumylhydrazine chloride
Cas No: 16227-10-4
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
triazbutil
Cas No: 16227-10-4
No Data 1 Gram 1000 Kilogram/Day CHANGCHUN WEIERSI IMPORT AND EXPORT TRADE CO.,LTD Contact Supplier
4H-1,2,4-Triazole,4-butyl-
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No Data No Data 10000 Metric Ton/Month Henan Wentao Chemical Product Co., Ltd. Contact Supplier
Factory Supply 4-butyl-1,2,4-triazole
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4H-1,2,4-Triazole,4-butyl-
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16227-10-4
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4-Butyl-4H-1,2,4-triazole/16227-10-4
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FENBUCONAZOLE
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4H-1,2,4-Triazole,4-butyl-
Cas No: 16227-10-4
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16227-10-4 Usage

InChI:InChI=1/C40H32N8O2.2ClH/c1-49-37-27-31(23-25-35(37)47-43-39(29-15-7-3-8-16-29)41-45(47)33-19-11-5-12-20-33)32-24-26-36(38(28-32)50-2)48-44-40(30-17-9-4-10-18-30)42-46(48)34-21-13-6-14-22-34;;/h3-28H,1-2H3;2*1H/q+2;;/p-2

16227-10-4SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 17, 2017

Revision Date: Aug 17, 2017

1.Identification

1.1 GHS Product identifier

Product name triazbutil

1.2 Other means of identification

Product number -
Other names 4-butyl-{1,2,4}triazole

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:16227-10-4 SDS

16227-10-4Synthetic route

1,2,4-Triazole
288-88-0

1,2,4-Triazole

1-bromo-butane
109-65-9

1-bromo-butane

A

1-butyl-1H-[1,2,4]triazole
6086-22-2

1-butyl-1H-[1,2,4]triazole

B

4-n-butyl-1,2,4-triazole
16227-10-4

4-n-butyl-1,2,4-triazole

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 0 - 20℃; Alkylation;A 85%
B n/a
With aluminum oxide; potassium fluoride; tetrabutylammomium bromide for 24h; Ambient temperature; Yield given. Yields of byproduct given;
With sodium hydroxide In N,N-dimethyl-formamide at 20℃; Alkylation;
1,2,4-Triazole
288-88-0

1,2,4-Triazole

1-bromo-butane
109-65-9

1-bromo-butane

A

1-butyl-1H-[1,2,4]triazole
6086-22-2

1-butyl-1H-[1,2,4]triazole

B

4-n-butyl-1,2,4-triazole
16227-10-4

4-n-butyl-1,2,4-triazole

C

1,4-dibutyl-4H-1,2,4-triazol-1-ium bromide

1,4-dibutyl-4H-1,2,4-triazol-1-ium bromide

Conditions
ConditionsYield
With lithium hydroxide; tetrabutylammomium bromide for 24h; Product distribution; Ambient temperature; also benzotriazole; other alkyl halides; var. base as reagents; also reactions in the absence of base; var. temperatures and reaction time; also with conventional heating or microwave heating instead of phase transfer catalysis;
N-butylamine
109-73-9

N-butylamine

orthoformic acid triethyl ester
122-51-0

orthoformic acid triethyl ester

formic acid hydrazide
624-84-0

formic acid hydrazide

4-n-butyl-1,2,4-triazole
16227-10-4

4-n-butyl-1,2,4-triazole

Conditions
ConditionsYield
Stage #1: orthoformic acid triethyl ester; formic acid hydrazide In methanol Heating;
Stage #2: N-butylamine In methanol Heating; Further stages.;
1,2,4-Triazole
288-88-0

1,2,4-Triazole

Dibutyl carbonate
542-52-9

Dibutyl carbonate

4-n-butyl-1,2,4-triazole
16227-10-4

4-n-butyl-1,2,4-triazole

Conditions
ConditionsYield
With magnesium carbonate at 200℃; for 20h; Inert atmosphere;5.25 g
methyl bromide
74-83-9

methyl bromide

4-n-butyl-1,2,4-triazole
16227-10-4

4-n-butyl-1,2,4-triazole

4-butyl-1-methyl-4H-1,2,4-triazol-1-ium bromide
1268852-02-3

4-butyl-1-methyl-4H-1,2,4-triazol-1-ium bromide

Conditions
ConditionsYield
In acetonitrile for 36h; Reflux; Inert atmosphere; Schlenk technique;96%
t-butyl bromide
507-19-7

t-butyl bromide

4-n-butyl-1,2,4-triazole
16227-10-4

4-n-butyl-1,2,4-triazole

4-butyl-1-tert-butyl-4H-1,2,4-triazol-1-ium bromide

4-butyl-1-tert-butyl-4H-1,2,4-triazol-1-ium bromide

Conditions
ConditionsYield
In acetonitrile for 36h; Reflux; Inert atmosphere; Schlenk technique;92%
4-n-butyl-1,2,4-triazole
16227-10-4

4-n-butyl-1,2,4-triazole

BH2(C2H2N3(C4H9))2(1+)*I(1-)=[BH2(C2H2N3(C4H9))2]I
1343472-85-4

BH2(C2H2N3(C4H9))2(1+)*I(1-)=[BH2(C2H2N3(C4H9))2]I

Conditions
ConditionsYield
With trimethylamine-borane; iodine In toluene for 24h; Reflux;85.8%
trimethylamine-borane
75-22-9

trimethylamine-borane

iodine
7553-56-2

iodine

4-n-butyl-1,2,4-triazole
16227-10-4

4-n-butyl-1,2,4-triazole

BH2(C2H2N3(C4H9))2(1+)*I(1-)=[BH2(C2H2N3(C4H9))2]I
1343472-85-4

BH2(C2H2N3(C4H9))2(1+)*I(1-)=[BH2(C2H2N3(C4H9))2]I

Conditions
ConditionsYield
In toluene I2 added to toluene soln. of Me3NBH3 , stirred at room temp. for 1 h, ligand added (1:2:4 molar ratio), mixt. refluxed for 24 h; filtered off, washed (hexane, Et2O, toluene), dried (80°C, vac.),recrystd. (hot EtOH), elem. anal.;85.8%
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