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7553-56-2 Usage

InChI:InChI=1/I2/c1-2

7553-56-2 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
TCI America (I0604)  Iodine  >98.0%(T) 7553-56-2 25g 145.00CNY Detail
TCI America (I0604)  Iodine  >98.0%(T) 7553-56-2 500g 520.00CNY Detail
Alfa Aesar (14312)  Iodine spheres, ultra dry, -10 mesh, 99.998% (metals basis)    7553-56-2 5g 817.0CNY Detail
Alfa Aesar (14312)  Iodine spheres, ultra dry, -10 mesh, 99.998% (metals basis)    7553-56-2 25g 3717.0CNY Detail
Alfa Aesar (14312)  Iodine spheres, ultra dry, -10 mesh, 99.998% (metals basis)    7553-56-2 100g 15816.0CNY Detail
Alfa Aesar (35636)  Iodine, 0.01N Standardized Solution    7553-56-2 1L 227.0CNY Detail
Alfa Aesar (35636)  Iodine, 0.01N Standardized Solution    7553-56-2 4L 588.0CNY Detail
Alfa Aesar (35634)  Iodine, 0.1N Standardized Solution    7553-56-2 1L 435.0CNY Detail
Alfa Aesar (35634)  Iodine, 0.1N Standardized Solution    7553-56-2 4L 1439.0CNY Detail
Alfa Aesar (35632)  Iodine, 1.0N Standardized Solution    7553-56-2 500ml 911.0CNY Detail
Alfa Aesar (35632)  Iodine, 1.0N Standardized Solution    7553-56-2 1L 1967.0CNY Detail
Alfa Aesar (44488)  Iodine, 1.0N Standardized Solution in ethanol    7553-56-2 1L 1803.0CNY Detail

7553-56-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 16, 2017

Revision Date: Aug 16, 2017

1.Identification

1.1 GHS Product identifier

Product name Iodine

1.2 Other means of identification

Product number -
Other names IODUM

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Inorganic substances, Metals/Elements (the simplest forms of matter), Radionuclides (radioactive materials)
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:7553-56-2 SDS

7553-56-2Synthetic route

sodium iodide
7681-82-5

sodium iodide

iodine
7553-56-2

iodine

Conditions
ConditionsYield
With phosgene In acetone at 20℃; for 0.25h; Reagent/catalyst;100%
With Fe3+-montmorillonite; propionic acid at 25℃; for 6h;
With propionic acid; K 10-montmorillonite; FeCl3; mixture of, dried at 120 degrees C, grounded at 25℃; for 6h;
hydrogen iodide
10034-85-2

hydrogen iodide

A

hydrogen
1333-74-0

hydrogen

B

iodine
7553-56-2

iodine

Conditions
ConditionsYield
Kinetics; Irradiation (UV/VIS); in glass vessel or uviol vessel, wavelenght higher than 2540Å;;A 100%
B 100%
Kinetics; Irradiation (UV/VIS); at room temperature, in quartz vessel; equilibrium; wavelenght lower than 2540Å;;A 92.3%
B 92.3%
995 °C; part of a Mg-S-I water splitting cycle;A 31%
B 31%
niobocene dichloride
12793-14-5

niobocene dichloride

triiodo hexafluoroarsenate
59555-19-0

triiodo hexafluoroarsenate

A

(η5-C5H5)2niobium(V)(Cl2) hexafluoroarsenate

(η5-C5H5)2niobium(V)(Cl2) hexafluoroarsenate

B

iodine
7553-56-2

iodine

Conditions
ConditionsYield
In liquid sulphur dioxide under Ar; recrystn. (SO2), elem. anal.;A 99%
B n/a
molybdenum(VI) oxide

molybdenum(VI) oxide

magnesium iodide

magnesium iodide

A

magnesium oxide * molybdenum dioxide

magnesium oxide * molybdenum dioxide

B

iodine
7553-56-2

iodine

C

magnesium oxide

magnesium oxide

Conditions
ConditionsYield
In neat (no solvent, solid phase) vac.; equimolar ratio, heating (200°C 20 d, 800°C 30 d); XRD;A n/a
B 98.5%
C n/a
bis(pyridine)iodine(I) tetrachloroplatinate(II)

bis(pyridine)iodine(I) tetrachloroplatinate(II)

A

{Pt(pyridinium)2Cl4}

{Pt(pyridinium)2Cl4}

B

iodine
7553-56-2

iodine

Conditions
ConditionsYield
In neat (no solvent, solid phase) byproducts: pyridine; heated at 130°C; washed with acetone-water (5:1), dried in vac.; elem. anal.;A 94%
B 96.5%
dimethoxy disulfide
28752-21-8

dimethoxy disulfide

A

iodine
7553-56-2

iodine

B

sulfur
7704-34-9

sulfur

Conditions
ConditionsYield
With hydrogenchloride byproducts: H2O, H2S, SO2; in presence of KI;A 90%
B n/a
With HCl byproducts: H2O, H2S, SO2; in presence of KI;A 90%
B n/a
bis(pyridine)iodine(I) tetrabromoplatinate(II)

bis(pyridine)iodine(I) tetrabromoplatinate(II)

B

iodine
7553-56-2

iodine

Conditions
ConditionsYield
In neat (no solvent, solid phase) byproducts: pyridine; heated at 120°C; washed with acetone-water (5:1), dried in vac.; elem. anal.;A 85%
B 72.7%
iodide
14362-44-8

iodide

iodine
7553-56-2

iodine

Conditions
ConditionsYield
With ammonium peroxosulfate; iron(III) In hydrogenchloride byproducts: SO4(2-); Irradiation (UV/VIS); at 22°C with UV irradiation for 15 min; subsequent stirring in daylight for 20 min; mechanism discussed;;80.2%
With ammonium peroxosulfate; iron(III) In hydrogenchloride byproducts: SO4(2-); at 22°C in daylight for 35 min;;73.9%
With ammonium peroxosulfate; iron(III) In hydrogenchloride byproducts: SO4(2-); at 22°C in the dark for 15 min; subsequent stirring in daylight for 20 min;;69.6%
bismuth (III) nitrate pentahydrate

bismuth (III) nitrate pentahydrate

iodic acid
7782-68-5

iodic acid

A

2Bi(3+)*IO4(3-)*3IO3(1-)=Bi2(IO4)(IO3)3

2Bi(3+)*IO4(3-)*3IO3(1-)=Bi2(IO4)(IO3)3

B

iodine
7553-56-2

iodine

Conditions
ConditionsYield
With HNO3 or I2O5 or H5IO6 In water High Pressure; mixt. of Bi compd., HIO3, HNO3 (or I2O5 or H5IO6) and H2O was sealed in autoclave; heated to 215°C; held for 5 d; cooled at rate 10°C/h to room temp.; decanted; washed (EtOH, H2O); air-dried;A 75%
B n/a
C8H7ClN4O

C8H7ClN4O

but-3-en-1-amine hydrochloride
17875-18-2

but-3-en-1-amine hydrochloride

iodine
7553-56-2

iodine

Conditions
ConditionsYield
With triethylamine In ethanol for 4h;74%
iodine pentoxide
12029-98-0

iodine pentoxide

potassium chloride

potassium chloride

uranium(VI) trioxide

uranium(VI) trioxide

A

K2((UO2)3(IO3)4O2)

K2((UO2)3(IO3)4O2)

B

iodine
7553-56-2

iodine

Conditions
ConditionsYield
In water High Pressure; UO2, I2O5, KCl, and water were heated in autoclave at 10°C/min to425°C, after 72 h autoclave was cooled over 24 h to 23°C; washed with MeOH and dried;A 73%
B n/a
N,N,N',N'-tetraethylthioamine
3768-61-4

N,N,N',N'-tetraethylthioamine

iodine
7553-56-2

iodine

Conditions
ConditionsYield
In not given in acidic soln.;70%
In not given in acidic soln.;70%
N-trifluoroacetic-3-nitroaniline
25080-83-5

N-trifluoroacetic-3-nitroaniline

methyl iodide
74-88-4

methyl iodide

iodine
7553-56-2

iodine

Conditions
ConditionsYield
Stage #1: N-trifluoroacetic-3-nitroaniline With sodium hydride In tetrahydrofuran at 0℃; for 1h;
Stage #2: methyl iodide In tetrahydrofuran at 20℃;
66%
iodine pentoxide
12029-98-0

iodine pentoxide

water
7732-18-5

water

uranium(VI) trioxide

uranium(VI) trioxide

barium(II) chloride

barium(II) chloride

A

uranyl iodate monohydrate

uranyl iodate monohydrate

B

Ba((UO2)2(IO3)2O2)*H2O

Ba((UO2)2(IO3)2O2)*H2O

C

iodine
7553-56-2

iodine

Conditions
ConditionsYield
In water High Pressure; UO2, I2O5, KCl, and water were heated in autoclave to 180°C, after 72 h autoclave was cooled at 9°C/h to 23°C; washed with MeOH and dried;A n/a
B 60%
C n/a
1,2-Diiodobenzene
615-42-9

1,2-Diiodobenzene

boron triiodide
13517-10-7

boron triiodide

A

iodine
7553-56-2

iodine

B

5,10-diiodo-5,10-dihydroboranthrene
24633-37-2

5,10-diiodo-5,10-dihydroboranthrene

Conditions
ConditionsYield
stirring mixt. of educts at 180°C for 5 h; I2 removed by sublimation at 60°C/0.1 Torr, sublimation of products;A n/a
B 56%
cyanogen iodide
506-78-5

cyanogen iodide

tertamethylammonium iodide
75-58-1

tertamethylammonium iodide

iodine
7553-56-2

iodine

Conditions
ConditionsYield
In neat (no solvent) at room temp.;38%
silver(I) iodide

silver(I) iodide

iodine
7553-56-2

iodine

Conditions
ConditionsYield
in presence of O3 at room temp.;2.8%
in presence of O3 at room temp.;2.8%
With manganese(IV) oxide at 370°C;
potassium iodate
7758-05-6

potassium iodate

A

iodine
7553-56-2

iodine

B

potassium iodide
7681-11-0

potassium iodide

Conditions
ConditionsYield
potassium polymanganite(IV) In solid byproducts: O2; mixt. of KIO3 and potassium polymanganate heated (400-600°C, 2h, air); X-ray diffraction;A 1%
B n/a
2-(iodomethyl)isoindoline-1,3-dione
203255-55-4

2-(iodomethyl)isoindoline-1,3-dione

iodine
7553-56-2

iodine

Conditions
ConditionsYield
Zerstzung bei Raumtemperatur;
2,4-dichloro-6-diiodomethyl-[1,3,5]triazine
30894-70-3

2,4-dichloro-6-diiodomethyl-[1,3,5]triazine

iodine
7553-56-2

iodine

Conditions
ConditionsYield
at 25℃;
8-iodo-3,7-dihydro-purine-2,6-dione
64761-27-9

8-iodo-3,7-dihydro-purine-2,6-dione

iodine
7553-56-2

iodine

Conditions
ConditionsYield
at 200℃; Abspaltung;
5,7-Diiodoisatin
34058-26-9

5,7-Diiodoisatin

sulfuric acid
7664-93-9

sulfuric acid

iodine
7553-56-2

iodine

Conditions
ConditionsYield
at 130℃; Zersetzung;
sulfuric acid
7664-93-9

sulfuric acid

2-iodo-1-(4-naphtho[1,2-d][1,2,3]triazol-2-yl-phenyl)-ethanone

2-iodo-1-(4-naphtho[1,2-d][1,2,3]triazol-2-yl-phenyl)-ethanone

iodine
7553-56-2

iodine

1-bromopyrrolidin-2-one
2401-40-3

1-bromopyrrolidin-2-one

hydrogen iodide
10034-85-2

hydrogen iodide

iodine
7553-56-2

iodine

(1R)-3-bromo-1,8,8-trimethyl-3-aza-bicyclo[3.2.1]octane-2,4-dione
128475-96-7

(1R)-3-bromo-1,8,8-trimethyl-3-aza-bicyclo[3.2.1]octane-2,4-dione

hydrogen iodide
10034-85-2

hydrogen iodide

iodine
7553-56-2

iodine

(1R)-3-iodo-1,8,8-trimethyl-3-aza-bicyclo[3.2.1]octane-2,4-dione

(1R)-3-iodo-1,8,8-trimethyl-3-aza-bicyclo[3.2.1]octane-2,4-dione

hydrogen iodide
10034-85-2

hydrogen iodide

iodine
7553-56-2

iodine

3-imino-2-phenyl-3H-indole
6339-33-9

3-imino-2-phenyl-3H-indole

water
7732-18-5

water

hydrogen iodide
10034-85-2

hydrogen iodide

iodine
7553-56-2

iodine

2,3,4,5-tetraiodo-1H-pyrrole
87-58-1

2,3,4,5-tetraiodo-1H-pyrrole

acetic anhydride
108-24-7

acetic anhydride

iodine
7553-56-2

iodine

sulfuric acid
7664-93-9

sulfuric acid

(3S)-cis-3,6-bis-(2,5-diiodo-1(3)H-imidazol-4-ylmethyl)-piperazine-2,5-dione

(3S)-cis-3,6-bis-(2,5-diiodo-1(3)H-imidazol-4-ylmethyl)-piperazine-2,5-dione

iodine
7553-56-2

iodine

Conditions
ConditionsYield
at 150℃;
sulfur dioxide
7446-09-5

sulfur dioxide

water
7732-18-5

water

iodine
7553-56-2

iodine

A

sulfuric acid
7664-93-9

sulfuric acid

B

hydrogen iodide
10034-85-2

hydrogen iodide

Conditions
ConditionsYield
0 - 25 °C; part of a Mg-S-I water splitting cycle;A 100%
B 100%
bromine
7726-95-6

bromine

iodine
7553-56-2

iodine

cadmium(II) sulphide

cadmium(II) sulphide

cadmium(II) iodide

cadmium(II) iodide

Conditions
ConditionsYield
In gas100%
In solid100%
In further solvent(s) with I2 dissolved in organic solvents;100%
bismuth
7440-69-9

bismuth

iodine
7553-56-2

iodine

bismuth(III) iodide
7787-64-6

bismuth(III) iodide

Conditions
ConditionsYield
In melt passing a stream of I2/inert gas into molten Bi with formation of volatile BiI3; description of the aparatus given;;100%
In melt passing a stream of I2/inert gas into molten Bi with formation of volatile BiI3; description of the aparatus given;;100%
In melt passing a stream of I2/inert gas into molten Bi with formation of volatile BiI3; description of the aparatus given;;100%
thallium

thallium

iodine
7553-56-2

iodine

thallium(I) iodide

thallium(I) iodide

Conditions
ConditionsYield
In neat (no solvent) in vac., for 0% excess Tl at 540°C, for 1% excess Tl at 500, 540°C, for 2, 5, 10, 20% excess Tl at 450, 500, 540°C; sublimed, elem. anal., IR, XRD;100%
In neat (no solvent) in vac., for 20% excess Tl at 400°C; sublimed, elem. anal., IR, XRD;99.1%
In neat (no solvent) in vac., for 0% excess Tl at 500°C; sublimed, elem. anal., IR, XRD;98.9%
lithium borohydride

lithium borohydride

iodine
7553-56-2

iodine

diborane
14452-61-0

diborane

Conditions
ConditionsYield
Kinetics; byproducts: H2, LiI; Interaction of initial cryst. materials in molar ratio LiBH4:I2 = 1.50 under mechanical activation with a vibration ball mill (dry N2, atm. pressure, 25°C).; Detn. of gas phase formed by infrared and mass spectroscopy, and gas volumetric anal.;100%
byproducts: H2, LiI; Interaction of initial cryst. materials in molar ratio LiBH4:I2 = 1.35 under mechanical activation with a vibration ball mill (dry N2, atm. pressure, 25°C).; Detn. of gas phase formed by infrared and mass spectroscopy, and gas volumetric anal.;99.5%
Kinetics; byproducts: H2, LiI; Interaction of initial cryst. materials in molar ratio LiBH4:I2 = 2.0 under mechanical activation with a vibration ball mill (dry N2, atm. pressure, 25°C).; Detn. of gas phase formed by infrared and mass spectroscopy, and gas volumetric anal.;99.8%
Kinetics; byproducts: H2, LiI; Interaction of initial cryst. materials in molar ratio LiBH4:I2 = 2.5 under mechanical activation with a vibration ball mill (dry N2, atm. pressure, 25°C).; Detn. of gas phase formed by infrared and mass spectroscopy, and gas volumetric anal.;95.4%
byproducts: H2, HI; Grinding of initial materials (molar ratio = 1) while being cooled withliq. N2, thorough mixing, transferring of mixt. to a thermographic ampoule and heating in vac. or N2.; Sepn. of gas mixt. by fractional condensation. Detn. of composition after the thermography by gas volumetric anal.;
sodium tetrahydroborate
16940-66-2

sodium tetrahydroborate

iodine
7553-56-2

iodine

diborane
14452-61-0

diborane

Conditions
ConditionsYield
byproducts: H2, NaI; Interaction of initial cryst. materials in molar ratio NaBH4:I2 = 1.35 under mechanical activation with a vibration ball mill (dry N2, atm. pressure, 25°C).; Detn. of gas phase formed by infrared and mass spectroscopy, and gas volumetric anal.;100%
byproducts: H2, NaI; Interaction of initial cryst. materials in molar ratio NaBH4:I2 = 1.5 under mechanical activation with a vibration ball mill (dry N2, atm. pressure, 25°C).; Detn. of gas phase formed by infrared and mass spectroscopy, and gas volumetric anal.;97.7%
Kinetics; byproducts: H2, NaI; Interaction of initial cryst. materials in molar ratio NaBH4:I2 = 2.5 under mechanical activation with a vibration ball mill (dry N2, atm. pressure, 25°C).; Detn. of gas phase formed by infrared and mass spectroscopy, and gas volumetric anal.;94%
Kinetics; byproducts: H2, NaI; Interaction of initial cryst. materials in molar ratio NaBH4:I2 = 2.0 under mechanical activation with a vibration ball mill (dry N2, atm. pressure, 25°C).; Detn. of gas phase formed by infrared and mass spectroscopy, and gas volumetric anal.;88.7%
byproducts: H2, HI; Grinding of initial materials (molar ratio = 1) while being cooled withliq. N2, thorough mixing, transferring of mixt. to a thermographic ampoule and heating in vac. or N2.; Sepn. of gas mixt. by fractional condensation. Detn. of composition after the thermography by gas volumetric anal.;
tellurium

tellurium

iodine
7553-56-2

iodine

tungsten(VI) chloride
13283-01-7

tungsten(VI) chloride

1,4-diiodo-cyclo-hexatellurium(2+) bis(hexachlorotungstate(-))

1,4-diiodo-cyclo-hexatellurium(2+) bis(hexachlorotungstate(-))

Conditions
ConditionsYield
In neat (no solvent) Ar atmosphere, sealed ampoule, formation of black melt at 300°C, tube furnace (150°C), crystn. (3 months);100%
cis-I(CO)2(CH3NC)2W.tplbond.CNEt2

cis-I(CO)2(CH3NC)2W.tplbond.CNEt2

iodine
7553-56-2

iodine

(I)3(CO)(CH3NC)2W.tplbond.CNEt2

(I)3(CO)(CH3NC)2W.tplbond.CNEt2

Conditions
ConditionsYield
In dichloromethane first at -30°c, than at room temp. for 10min stirring, reducing of the soln., adding Et2O/pentane; drying at 25°C (vacuo), elem. anal.;100%
cis-{(PhCH2)2Co(III)(2,2'-bipyridine)2}ClO4

cis-{(PhCH2)2Co(III)(2,2'-bipyridine)2}ClO4

iodine
7553-56-2

iodine

cis-benzyl iodo bis(2,2'-bipyridyl) cobalt(III) perchlorate

cis-benzyl iodo bis(2,2'-bipyridyl) cobalt(III) perchlorate

B

iodomethylbenzene
620-05-3

iodomethylbenzene

Conditions
ConditionsYield
In tetrachloromethane Kinetics; Irradiation (UV/VIS); Kinetics of the reaction of Co(H2CC6H5)2(bipy)2ClO4 with I2 under irradiation with light at 517 nm is investigated.; PhCh2I and Co(H2CC6H5)I(bipy)2ClO4 are the main products.;A n/a
B 100%
trans-(CH3)2Co(11-hydroxy-2,3,9,10-tetramethyl-1,4,8,11-tetraazaundeca-1,3,8,10-tetraen-1-olate)

trans-(CH3)2Co(11-hydroxy-2,3,9,10-tetramethyl-1,4,8,11-tetraazaundeca-1,3,8,10-tetraen-1-olate)

iodine
7553-56-2

iodine

A

methane
34557-54-5

methane

B

ethane
74-84-0

ethane

C

methyl iodide
74-88-4

methyl iodide

Conditions
ConditionsYield
In tetrachloromethane Irradiation (UV/VIS); Irradiation at 509 nm in CCl4; Estimation of the quantum yield of the photochemical reaction. Yield of the products estimated by g.l.c.;A 0.02%
B <1
C 100%
trans-(CH3)2Co(11-hydroxy-2,3,9,10-tetramethyl-1,4,8,11-tetraazaundeca-1,3,8,10-tetraen-1-olate)

trans-(CH3)2Co(11-hydroxy-2,3,9,10-tetramethyl-1,4,8,11-tetraazaundeca-1,3,8,10-tetraen-1-olate)

iodine
7553-56-2

iodine

trans-methyl iodo cobalt (III) 3,9-dimethyl-4,8-diazaundecane-3,8-diene-2,10-dione dioximate

trans-methyl iodo cobalt (III) 3,9-dimethyl-4,8-diazaundecane-3,8-diene-2,10-dione dioximate

B

methyl iodide
74-88-4

methyl iodide

Conditions
ConditionsYield
In tetrachloromethane Kinetics; byproducts: C2H6, CH4; Irradiation (UV/VIS); Kinetics of the reaction of Co(CH3)2(H3CCNOHC(CH3)NC3H6NC(CH3)CNOCH3) with I2 under irradiation with light at 517 nm is investigated.; MeI and Co(CH3)I(H3CCNOHC(CH3)NC3H6NC(CH3)CNOCH3) are the main products, C2H6 and CH4 are byproducts.;A n/a
B 100%
CoMe(pyridine)(dimethylglyoxime(-1H))2
23642-14-0

CoMe(pyridine)(dimethylglyoxime(-1H))2

iodine
7553-56-2

iodine

A

iodobisdimethylglyoximepyridine cobalt(III)

iodobisdimethylglyoximepyridine cobalt(III)

B

methyl iodide
74-88-4

methyl iodide

Conditions
ConditionsYield
In tetrachloromethane Kinetics; Irradiation (UV/VIS); Kinetics of the reaction of Co(CH3)(H3CCNOHONCCH3)2(C5H5N) with I2 under irradiation with light at 517 nm is investigated.; MeI and CoI(H3CCNOHONCCH3)2(C5H5N) are the products.;A n/a
B 100%
[CoEt(dimethylglyoximate(1-))2(pyridine)]

[CoEt(dimethylglyoximate(1-))2(pyridine)]

iodine
7553-56-2

iodine

A

iodobisdimethylglyoximepyridine cobalt(III)

iodobisdimethylglyoximepyridine cobalt(III)

B

ethyl iodide
75-03-6

ethyl iodide

Conditions
ConditionsYield
In tetrachloromethane Kinetics; Irradiation (UV/VIS); Kinetics of the reaction of Co(C2H5)(H3CCNOHONCCH3)2(C5H5N) with I2 under irradiation with light at 517 nm is investigated.; MeI and CoI(H3CCNOHONCCH3)2(C5H5N) are the products.;A n/a
B 100%
(η4-2,5-bis(trimethylsilyl)-3,4-cyclopentacyclopentadienone)(η5-cyclopentadienyl)cobalt

(η4-2,5-bis(trimethylsilyl)-3,4-cyclopentacyclopentadienone)(η5-cyclopentadienyl)cobalt

iodine
7553-56-2

iodine

(η4-2-iodo-5-trimethylsilyl-3,4-cyclopentacyclopentadienone)(η5-cyclopentadienyl)cobalt

(η4-2-iodo-5-trimethylsilyl-3,4-cyclopentacyclopentadienone)(η5-cyclopentadienyl)cobalt

Conditions
ConditionsYield
With sodium thiosulfate In acetone addn. of iodine to a soln. of Co-compd., stirring at room temp. for 1 h, change of colour from brown-red to red on addn. of aq. Na2S2O3; extg. the aq. layer with CH2Cl2, drying over Na2SO4, filtration, evapn., chromy. (Al2O3, ethyl acetate), elem. anal.;100%
Pt2I2(CO)2(P-tert.-Bu2Ph2)2
118714-49-1

Pt2I2(CO)2(P-tert.-Bu2Ph2)2

iodine
7553-56-2

iodine

PtPtI2(CO)(P-t-Bu2Ph)
19618-88-3

PtPtI2(CO)(P-t-Bu2Ph)

Conditions
ConditionsYield
In not given react. (N2, CO or Ar); elem. anal.;100%
iodine
7553-56-2

iodine

triethylantimony
617-85-6

triethylantimony

triethylstibine di-iodide
25088-65-7, 58116-52-2

triethylstibine di-iodide

Conditions
ConditionsYield
In dichloromethane elem. anal.;100%
selenium
7782-49-2

selenium

arsenic pentafluoride
7784-36-3

arsenic pentafluoride

fluorosulfonylchloride
13637-84-8

fluorosulfonylchloride

sulfur dioxide
7446-09-5

sulfur dioxide

iodine
7553-56-2

iodine

(diselenium tetraiodine)(AsF6)2*SO2

(diselenium tetraiodine)(AsF6)2*SO2

Conditions
ConditionsYield
byproducts: AsF3; SO2 and AsF5 were condensed into Se and I2; after 16 h no insoluble material was observed; condensed SO2ClF into the soln.; react. time 3 h; slowly (ca.20 h) condension; cooling; crystn.; washing; removed volatile materials by evacuation; subjected to vac. for <0.2 h; elem. anal.;100%
byproducts: AsF3; SO2 and AsF5 were condensed onto Se and I2; after 16 h no insoluble material was observed; condensation of SO2ClF onto the soln.; react. time 7 h; slowly (ca.20 h) condensation of solvent; cooling; crystn.; washing; removal of volatile material by evacuation; elem. anal.;104 %
selenium
7782-49-2

selenium

arsenic pentafluoride
7784-36-3

arsenic pentafluoride

sulfur dioxide
7446-09-5

sulfur dioxide

iodine
7553-56-2

iodine

(diselenium tetraiodine)-(AsF6)2

(diselenium tetraiodine)-(AsF6)2

Conditions
ConditionsYield
AsF5 was condensed onto a mixture of Se and I2 in liq. SO2; react. time 4 h; slowly (ca.20 h) condensation of solvent; crystn.; after 16 h removal of volatile material by evacuation; elem. anal.; X-ray diffraction;100%
AsF5 was condensed onto a mixture of Se and I2 in liq. SO2; react. time 6 h; slowly (ca.20 h) condensation; crystn.; after 16 h removal of volatile materials by evacuation; elem. anal.; X-ray diffraction;106 %
anti-2-norbornene-7-yl-trimethyl tin
38573-93-2, 34208-81-6

anti-2-norbornene-7-yl-trimethyl tin

iodine
7553-56-2

iodine

trimethylstannyl iodide
811-73-4

trimethylstannyl iodide

Conditions
ConditionsYield
In methanol100%
In methanol100%
In dimethyl sulfoxide88%
iodine
7553-56-2

iodine

methyl 3-(tri-n-butylstannyl)propionate
19464-44-9

methyl 3-(tri-n-butylstannyl)propionate

β-Methoxycarbonyl-ethyldi-n-butyl-iodstannan

β-Methoxycarbonyl-ethyldi-n-butyl-iodstannan

Conditions
ConditionsYield
In tetrachloromethane byproducts: CH3(CH2)3I;100%
benzimidazolin-2-ylidene(chloro)gold
136835-13-7

benzimidazolin-2-ylidene(chloro)gold

iodine
7553-56-2

iodine

(benzimidazolin-2-ylidene)triiodogold

(benzimidazolin-2-ylidene)triiodogold

Conditions
ConditionsYield
In dichloromethane protective gas: argon; stirring mixture (20 h/room temp.);; pptn.; filtration; washing (CH2Cl2); drying; elem. anal.;;100%
((C6H5)2PC5H4)Mo(CO)3Mn(CO)5
165751-19-9

((C6H5)2PC5H4)Mo(CO)3Mn(CO)5

iodine
7553-56-2

iodine

[(η5-C5H4PPh2)Mo(CO)3I]

[(η5-C5H4PPh2)Mo(CO)3I]

Conditions
ConditionsYield
In not given100%
{Ru(C5H3(OH)(P(C6H5)3))(C5H5)}(1+)*PF6(1-)={Ru(C5H3(OH)(P(C6H5)3))(C5H5)}PF6

{Ru(C5H3(OH)(P(C6H5)3))(C5H5)}(1+)*PF6(1-)={Ru(C5H3(OH)(P(C6H5)3))(C5H5)}PF6

iodine
7553-56-2

iodine

{Ru(C5H5)(C5H3OP(C6H5)3)I}(1+)*PF6(1-)={Ru(C5H5)(C5H3OP(C6H5)3)I}(PF6)

{Ru(C5H5)(C5H3OP(C6H5)3)I}(1+)*PF6(1-)={Ru(C5H5)(C5H3OP(C6H5)3)I}(PF6)

Conditions
ConditionsYield
In nitromethane-d3 not isolated, monitored by NMR;100%
iodine
7553-56-2

iodine

bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]distilbene
201533-93-9

bis[2,4,6-tris[bis(trimethylsilyl)methyl]phenyl]distilbene

[((Si(CH3)3)2CH)3C6H2]SbI2
201533-95-1

[((Si(CH3)3)2CH)3C6H2]SbI2

Conditions
ConditionsYield
In tetrachloromethane room temp.;100%
μ-carbido-bis(phthalocyaninato(2-)iron(IV))

μ-carbido-bis(phthalocyaninato(2-)iron(IV))

iodine
7553-56-2

iodine

0.34[(C32H16N8)Fe]2C*0.66[(C32H16N8)Fe]2C(1+)*0.66I3(1-)=([(C32H16N8)Fe]2C)(I3)066

0.34[(C32H16N8)Fe]2C*0.66[(C32H16N8)Fe]2C(1+)*0.66I3(1-)=([(C32H16N8)Fe]2C)(I3)066

Conditions
ConditionsYield
In further solvent(s) excess of I2, stirring in chloronaphthalene (60-70°C, 1 h); cooling, collection (filtration), washing (EtOH), drying (vac.); elem. anal.;100%
tetra(supersilyl)dialane
192053-32-0

tetra(supersilyl)dialane

iodine
7553-56-2

iodine

disupersilyl aluminum iodide
217202-48-7

disupersilyl aluminum iodide

Conditions
ConditionsYield
In pentane Ar-atmosphere; stirring (40°C, 3 h); detd. by NMR spectroscopy;100%
In pentane all manipulations with exclusion of air and moisture; soln. of compds. heated at 40°C for 3 h; controlled by NMR; volatiles evapd. by oil pump; elem. anal.;
phenyl bis(trifluoroacetate)

phenyl bis(trifluoroacetate)

iodine
7553-56-2

iodine

A

iodobenzene
591-50-4

iodobenzene

B

Tl(1+)*Tl(3+)*4CF3COO(1-)=Tl2(CF3COO)4

Tl(1+)*Tl(3+)*4CF3COO(1-)=Tl2(CF3COO)4

Conditions
ConditionsYield
In acetonitrile soln. of iodine addn. to soln. of Tl-compd., mixing, standing (dark, 220h, room temperature), evacuation (under Ar, room temperature, then wate r bath, distillation of I-compd.), product remaining in solid residue;A 99%
B 100%
tellurium

tellurium

iodine
7553-56-2

iodine

aluminium(III) iodide
7784-23-8

aluminium(III) iodide

TeI3(1+)*AlI4(1-)=TeI3[AlI4]
165602-57-3

TeI3(1+)*AlI4(1-)=TeI3[AlI4]

Conditions
ConditionsYield
In neat (no solvent) Ar atm.; molar ratio Te:I2:AlI3 1:2:1, heating (150-200°C, several hours);100%
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