18523-16-5

Basic information

• Product Name: 1,3,5-Trimethoxy-2,4,6-trinitrobenzene
• Synonyms: 1,3,5-Trimethoxy-2,4,6-trinitrobenzene
• CAS NO: 18523-16-5
• Molecular Weight: 303.185
• Mol File: 18523-16-5.mol
• Article Data: 8

Chemical Properties

• CAS DataBase Reference: 1,3,5-Trimethoxy-2,4,6-trinitrobenzene(CAS DataBase Reference)
• NIST Chemistry Reference: 1,3,5-Trimethoxy-2,4,6-trinitrobenzene(18523-16-5)
• EPA Substance Registry System: 1,3,5-Trimethoxy-2,4,6-trinitrobenzene(18523-16-5)

Safety Data

• Hazardous Substances Data: 18523-16-5(Hazardous Substances Data)

Upstream product

• 339199-98-3 1,3,5-trinitro-2,4,6-triphenoxy-benzene 
• 124-41-4 sodium methylate 
• 186581-53-3 diazomethane 
• 4328-17-0 trinitrophloroglucinol 
• 149-73-5 trimethyl orthoformate 
• 67-56-1 methanol 
• 107-31-3 Methyl formate 
• 1228939-33-0 5-methoxystyphnic acid 
• 621-23-8 1,2,3-trimethoxybenzene 
• 860556-89-4 3-chloro-1,5-dimethoxy-2,4-dinitro-benzene 
• 861081-00-7 1-chloro-3,5-dimethoxy-2,4-dinitro-benzene 
• 6284-83-9 1,3,5-trichloro-2,4-dinitrobenzene 
• 871880-52-3 1-chloro-3,5-dimethoxy-2,4,6-trinitrobenzene 
• 71-43-2 benzene 

Downstream Products

• 3058-38-6 2,4,6-triamino-1,3,5-trinitrobenzene 
• 132699-69-5 N,N',N''-Triisopropyl-2,4,6-trinitro-benzene-1,3,5-triamine; compound with isopropylamine 
• 132699-67-3 1,3,5-Tris<(2,2-dimethyl)propylamino>-2,4,6-trinitrobenzene 
• 68959-41-1 1,3,5-triethoxy-2,4,6-trinitrobenzene 

Relevant articles and documents

Preparation method of 1,3,5-trialkoxy-2,4,6-trinitrobenzene

The invention discloses a preparation method of 1,3,5-trimethoxy-2,4,6-trinitrobenzene. The method comprises the following steps: dissolving trinitrophloroglucinol in an alkylating reagent with the mass being 5 times that of the trinitrophloroglucinol to obtain a raw material solution; pumping the raw material solution into a continuous flow tubular reactor I, and reacting at 80-110 DEG C for 5-30 minutes to obtain an alkylation reaction solution; feeding the alkylation reaction liquid into a continuous flow tubular reactor II for cooling for 5-10 minutes, wherein the cooling temperature is 20-30 DEG C; and taking out the product, adding the product into a devitrification solution, and performing cooling, devitrifying, stirring, filtering and drying to obtain a product 1,3,5-trimethoxy-2,4,6-trinitrobenzene, wherein the alkylating reagent is a methylation reagent or an ethylation reagent or a propylation reagent. A continuous flow technology is used for inhibiting side reaction, the yield and purity of a target product are improved, and the post-treatment process is greatly simplified. The method can easily control reaction process and is suitable for industrial production.

Method for TORTNB etherification synthesis in microreactor

The invention discloses a method for TORTNB etherification synthesis in microreactor. The method includes steps: dissolving a nitrification product TNPG into an organic solvent; simultaneously pumpingTNPG solution and an etherification into a micro mixer,

Synthesis of trinitroaromatics using alternative mixed acid nitration conditions

Conditions for the mild and efficient nitration of phloroglucinol (1,3,5-trihydroxybenzene), 5-methoxyresorcinol, 3,5-dimethoxyphenol, and 1,3,5-trimethoxybenzene have been developed. Yields of the trinitro derivatives are excellent (～90%) for systems hav