1950-20-5Relevant academic research and scientific papers
Straightforward and highly efficient catalyst-free one-pot synthesis of dithiocarbamates under solvent-free conditions
Azizi, Najmedin,Aryanasab, Fezzeh,Saidi, Mohammad R.
, p. 5275 - 5277 (2007/10/03)
A highly efficient and simple synthesis of dithiocarbamates is possible based on the one-pot reaction of amines, CS2, and alkyl halides without using a catalyst under solvent-free conditions. The mild reaction conditions, high yields, and broad scope of the reaction illustrate the good synthetic utility of this method. The reaction is a highly atom-economic process for production of S-alkyl thiocarbamates and successfully can be used in high quantities in the pharmaceutical or agrochemical industries.
A simple one-pot preparation of dithiocarbamates in the presence of anhydrous potassium phosphate
Li, Run-Tao,Ding, Ping-Yu,Han, Mei,Cai, Meng-Shen
, p. 295 - 300 (2007/10/03)
Different kinds of dithiocarbamates were prepared by a simple one-pot procedure from primary or secondary amines, carbon disulfide and a variety of alkyl halides in the presence of anhydrous potassium phosphate under mild condition in good yields.
