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2-Ethylhexyl glycidyl ether
Cas No: 2461-15-6
USD $ 4.75-6.05 / Kilogram 1000 Kilogram 5000 Metric Ton/Year Anhui Xinyuan Technology Co.,Ltd Contact Supplier
2-Ethylhexyl glycidyl ether TOP1 supplier
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2-Ethylhexyl glycidyl ether CAS 2461-15-6 in stock 1,2-Epoxy-3-((2-ethylhexyl)oxy)propane
Cas No: 2461-15-6
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High quality 2-Ethylhexyl Glycidyl Ether supplier in China
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2-Ethylhexyl Glycidyl Ether
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Factory Supply 2-Ethylhexyl Glycidyl Ether
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2-(2-ethylhexoxymethyl)oxirane
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TIANFU-CHEM CAS:2461-15-6 2-Ethylhexyl glycidyl ether
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FactorysupplyEHGE/2-EthylhexylglycidyletherCAS2461-15-6
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2461-15-6 Usage

Chemical Properties

colourless liquid

General Description

Clear colorless liquid.

Fire Hazard

2-Ethylhexyl glycidyl ether is combustible.

Uses

It constitutes a reactive diluent and may be used as a relatively nonvolatile chloride-scavenging agent and stabilizer for vinyl resins and rubber.

Production Methods

2-Ethylhexyl glycidyl ether is made by condensation of 2-ethylhexanol with epichlorohydrin followed by dehydrochlorination with caustic to form the epoxy ring.

Air & Water Reactions

Insoluble in water.

Reactivity Profile

2-Ethylhexyl glycidyl ether is incompatible with acids, bases and oxidizing agents.
InChI:InChI=1/C11H22O2/c1-3-5-6-10(4-2)7-12-8-11-9-13-11/h10-11H,3-9H2,1-2H3

2461-15-6 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (251747)  2-Ethylhexylglycidylether  98% 2461-15-6 251747-250ML 999.18CNY Detail
Aldrich (251747)  2-Ethylhexylglycidylether  98% 2461-15-6 251747-1L 3,133.26CNY Detail

2461-15-6SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 11, 2017

Revision Date: Aug 11, 2017

1.Identification

1.1 GHS Product identifier

Product name 2-Ethylhexyl glycidyl ether

1.2 Other means of identification

Product number -
Other names (2-ethylhexyloxy)oxyran-2-ylmethane

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. CBI,Paint additives and coating additives not described by other categories
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:2461-15-6 SDS

2461-15-6Synthetic route

1-chloro-3-(2-ethyl-hexyloxy)-propan-2-ol
37961-18-5

1-chloro-3-(2-ethyl-hexyloxy)-propan-2-ol

2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran at 20 - 25℃; for 18h;
2-Ethylhexyl alcohol
104-76-7

2-Ethylhexyl alcohol

epichlorohydrin
106-89-8

epichlorohydrin

A

2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

B

1,3-di(2-ethylhexyloxy)-2-propylglycidyl ether

1,3-di(2-ethylhexyloxy)-2-propylglycidyl ether

C

3-chloroprop-2-enylglycidyl ether

3-chloroprop-2-enylglycidyl ether

Conditions
ConditionsYield
Stage #1: 2-Ethylhexyl alcohol With tetrabutylammomium bromide; sodium hydroxide at -40℃; for 0.5h; Inert atmosphere;
Stage #2: epichlorohydrin at 80℃; for 12h; Reagent/catalyst; Temperature;
2-Ethylhexyl alcohol
104-76-7

2-Ethylhexyl alcohol

epichlorohydrin
106-89-8

epichlorohydrin

2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

Conditions
ConditionsYield
Stage #1: 2-Ethylhexyl alcohol With tetrabutylammomium bromide; sodium hydroxide at -40℃; for 0.5h; Inert atmosphere;
Stage #2: epichlorohydrin at 40℃; for 12h; Reagent/catalyst; Temperature;
Stage #1: 2-Ethylhexyl alcohol; epichlorohydrin With sulfuric acid; (3-chloro-2-hydroxypropyl)-2-ethylhexyl ether at 80 - 100℃; for 4h;
Stage #2: With sodium hydroxide at 50℃;
Stage #3: With sodium chloride; sodium hydroxide In water at 85 - 95℃; for 6h;
752.8 g
2-Ethylhexyl alcohol
104-76-7

2-Ethylhexyl alcohol

epichlorohydrin
106-89-8

epichlorohydrin

A

2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

B

1,3-di(2-ethylhexyloxy)-2-propylglycidyl ether

1,3-di(2-ethylhexyloxy)-2-propylglycidyl ether

Conditions
ConditionsYield
Stage #1: 2-Ethylhexyl alcohol With tetrabutylammomium bromide; sodium hydroxide at -40℃; for 0.5h; Inert atmosphere;
Stage #2: epichlorohydrin at 60℃; for 12h; Reagent/catalyst; Temperature;
2-Ethylhexyl alcohol
104-76-7

2-Ethylhexyl alcohol

epichlorohydrin
106-89-8

epichlorohydrin

A

2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

B

5,13-diethyl-7,11-dioxa-9-heptadecanol
59068-03-0

5,13-diethyl-7,11-dioxa-9-heptadecanol

Conditions
ConditionsYield
Stage #1: 2-Ethylhexyl alcohol With tetrabutylammomium bromide; sodium hydroxide at -40℃; for 0.5h; Inert atmosphere;
Stage #2: epichlorohydrin at 40℃; for 12h; Reagent/catalyst; Temperature;
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

1-O-(2-ethylhexyl)glycerin
70445-33-9

1-O-(2-ethylhexyl)glycerin

Conditions
ConditionsYield
With formic acid; water; sodium hydroxide In Triethylene glycol dimethyl ether at 120℃; for 12h; Reagent/catalyst; Solvent;98.5%
Stage #1: 2-ethyl-hexyl glycidyl ether With boron trifluoride diethyl etherate In acetone at 10 - 20℃; for 2.66667h;
Stage #2: With methylamine In water; acetone at 10 - 20℃; for 0.166667h;
Stage #3: With formic acid In water at 50 - 55℃; for 3h; Temperature; Reagent/catalyst;
89.1%
Stage #1: 2-ethyl-hexyl glycidyl ether With formic acid; sulfuric acid at 80 - 100℃;
Stage #2: With methanol at 60℃;
Stage #3: With water; sodium hydroxide Product distribution / selectivity;
78.1%
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

3-(2-ethylhexoxy)propylamine
5397-31-9

3-(2-ethylhexoxy)propylamine

C33H69NO5

C33H69NO5

Conditions
ConditionsYield
at 60 - 120℃; for 10.67h;98%
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

2-(4-ethyl-2-oxaoctyl)thiirane
71242-04-1

2-(4-ethyl-2-oxaoctyl)thiirane

Conditions
ConditionsYield
With thiourea In methanol for 48h; Ambient temperature;97.4%
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

carbon dioxide
124-38-9

carbon dioxide

4-(((2-ethylhexyl)oxy)methyl)-1,3-dioxolan-2-one

4-(((2-ethylhexyl)oxy)methyl)-1,3-dioxolan-2-one

Conditions
ConditionsYield
With tetrabutylammomium bromide at 110℃; under 7500.75 Torr; for 3h;91%
With (2-aminoethyl)(4-(bis(2,6-dimethoxyphenyl)methylene)-3,5-dimethoxycyclohexa-2,5-dien-1-yl)diphenylphosphonium trifluoromethanesulfonate; sodium iodide In chlorobenzene at 100℃; under 760.051 Torr; for 12h; Schlenk technique;91%
With C24H12N2O10(4-)*2Cu(2+); tetrabutylammomium bromide at 20℃; under 760.051 Torr; for 48h; Schlenk technique;6%
2-Ethylhexylamine
104-75-6

2-Ethylhexylamine

2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

poly(2-ethylhexylamine-co-2-ethylhexyl glycidyl ether)

poly(2-ethylhexylamine-co-2-ethylhexyl glycidyl ether)

Conditions
ConditionsYield
at 60 - 120℃; for 10.6667h;90%
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

carbon monoxide
201230-82-2

carbon monoxide

2-hydroxybromobenzene
95-56-7

2-hydroxybromobenzene

3-(((2-ethylhexyl)oxy)methyl)-2H-benzo[e][1,4]dioxepin-5(3H)-one
1556674-22-6

3-(((2-ethylhexyl)oxy)methyl)-2H-benzo[e][1,4]dioxepin-5(3H)-one

Conditions
ConditionsYield
With potassium phosphate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In N,N-dimethyl-formamide at 100℃; under 3750.38 Torr; for 16h; Autoclave;88%
3-(dodecyloxy)-1-propylamine
7617-74-5

3-(dodecyloxy)-1-propylamine

2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

poly(2-ethylhexyl glycidyl ether-co-3-(dodecyloxy)-1-propylamine)

poly(2-ethylhexyl glycidyl ether-co-3-(dodecyloxy)-1-propylamine)

Conditions
ConditionsYield
at 60 - 120℃; for 10.6667h;85%
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

2-Ethylhexyl alcohol
104-76-7

2-Ethylhexyl alcohol

5,13-diethyl-7,11-dioxa-9-heptadecanol
59068-03-0

5,13-diethyl-7,11-dioxa-9-heptadecanol

Conditions
ConditionsYield
sulfated zirconium oxide at 150℃; Inert atmosphere;83.2%
With sodium hydride for 48h; Ambient temperature;61%
With tetrabutylammomium bromide; sodium hydroxide at 60℃; Cooling with ice;
carbon disulfide
75-15-0

carbon disulfide

2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

4-(4-ethyl-2-oxaoctyl)-1,3-dithiolane-2-thione

4-(4-ethyl-2-oxaoctyl)-1,3-dithiolane-2-thione

Conditions
ConditionsYield
With potassium hydroxide In methanol for 96h; Ambient temperature;82%
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

i-Amyl alcohol
123-51-3

i-Amyl alcohol

11-ethyl-2-methyl-5,9-dioxa-7-pentadecanol
93314-60-4

11-ethyl-2-methyl-5,9-dioxa-7-pentadecanol

Conditions
ConditionsYield
With sodium hydride for 48h; Ambient temperature;79%
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

4-(4,6-diphenyl-pyrimidin-2-yl)-benzene-1,3-diol
2915-23-3

4-(4,6-diphenyl-pyrimidin-2-yl)-benzene-1,3-diol

C33H38N2O4
163263-83-0

C33H38N2O4

Conditions
ConditionsYield
With ethyltriphenylphosphonium bromide at 150℃; for 0.5h;71.7%
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

(+/-)-2-methyl-1-butanol
137-32-6

(+/-)-2-methyl-1-butanol

11-ethyl-3-methyl-5,9-dioxa-7-pentadecanol
174719-45-0

11-ethyl-3-methyl-5,9-dioxa-7-pentadecanol

Conditions
ConditionsYield
With sodium hydride for 48h; Ambient temperature;69%
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

C9H9N*HO3S

C9H9N*HO3S

sulfuric acid mono-[2-(3,4-dihydro-isoquinolin-2-yl)-1-(2-ethyl-hexyloxymethy)-ethyl] ester

sulfuric acid mono-[2-(3,4-dihydro-isoquinolin-2-yl)-1-(2-ethyl-hexyloxymethy)-ethyl] ester

Conditions
ConditionsYield
at 75 - 80℃; for 72h; Product distribution / selectivity;68%
7,8-benzoquinoline
230-27-3

7,8-benzoquinoline

2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

1-(benzo[h]quinolin-10-yl)-3-((2-ethylhexyl)oxy)-2-propanol

1-(benzo[h]quinolin-10-yl)-3-((2-ethylhexyl)oxy)-2-propanol

Conditions
ConditionsYield
With 1,1,1,3',3',3'-hexafluoro-propanol; palladium diacetate; acetic acid at 25℃; for 24h; Inert atmosphere;58%
3,4-dihydroisoquinoline
3230-65-7

3,4-dihydroisoquinoline

2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

sulfuric acid mono-[2-(3,4-dihydro-isoquinolin-2-yl)-1-(2-ethyl-hexyloxymethy)-ethyl] ester

sulfuric acid mono-[2-(3,4-dihydro-isoquinolin-2-yl)-1-(2-ethyl-hexyloxymethy)-ethyl] ester

Conditions
ConditionsYield
In acetonitrile at 80℃; for 72h; Product distribution / selectivity;55%
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

3,4,9,10-perylenetetracarboxylic diimide bis(tetrabutylammonium) salt

3,4,9,10-perylenetetracarboxylic diimide bis(tetrabutylammonium) salt

C46H54N2O8

C46H54N2O8

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 100℃; for 10h; Inert atmosphere;50%
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

9-ethyl-5-(5-methyl-2-oxa-1-hexyl)-4,7-dioxa-1-tridecanesulfonic acid sodium salt

9-ethyl-5-(5-methyl-2-oxa-1-hexyl)-4,7-dioxa-1-tridecanesulfonic acid sodium salt

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 79 percent / sodium hydride / 48 h / Ambient temperature
2: 98 percent / sodium hydride / dimethylformamide / 3 h
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

12-ethyl-8-(5-methyl-2-oxa-1-hexyl)-4,7,10-trioxa-1-hexadecanesulfonic acid sodium salt

12-ethyl-8-(5-methyl-2-oxa-1-hexyl)-4,7,10-trioxa-1-hexadecanesulfonic acid sodium salt

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 79 percent / sodium hydride / 48 h / Ambient temperature
2: sodium hydride / acetonitrile / 0.5 h / Heating; before reflux 1 h room temperature
3: 1M HCl / 2 h / Heating
4: 100 percent / sodium hydride / dimethylformamide / 1 h / 60 °C
View Scheme
Multi-step reaction with 4 steps
1: 79 percent / sodium hydride / 48 h / Ambient temperature
2: 89 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
3: 1.) ozone, 2.) sodium borohydride / 1.) methanol, -78 deg C, 2.) methanol, to room temperature
4: 100 percent / sodium hydride / dimethylformamide / 1 h / 60 °C
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

6-ethyl-4-oxadecane-1,2-dithiol
174719-33-6

6-ethyl-4-oxadecane-1,2-dithiol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 97.4 percent / thiourea / methanol / 48 h / Ambient temperature
2: 37 percent / sodium hydrosulfide, hydrogen sulfide / ethanol / 3 h
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

8-ethyl-4-(4-methyl-2-oxa-1-hexyl)-3,6-dioxa-1-dodecanol
174719-47-2

8-ethyl-4-(4-methyl-2-oxa-1-hexyl)-3,6-dioxa-1-dodecanol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 69 percent / sodium hydride / 48 h / Ambient temperature
2: 93 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
3: 1.) ozone, 2.) sodium borohydride / 1.) methanol, -78 deg C, 2.) methanol, to room temperature
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

8-ethyl-4-(5-methyl-2-oxa-1-hexyl)-3,6-dioxa-1-dodecanol
174719-42-7

8-ethyl-4-(5-methyl-2-oxa-1-hexyl)-3,6-dioxa-1-dodecanol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 79 percent / sodium hydride / 48 h / Ambient temperature
2: sodium hydride / acetonitrile / 0.5 h / Heating; before reflux 1 h room temperature
3: 1M HCl / 2 h / Heating
View Scheme
Multi-step reaction with 3 steps
1: 79 percent / sodium hydride / 48 h / Ambient temperature
2: 89 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
3: 1.) ozone, 2.) sodium borohydride / 1.) methanol, -78 deg C, 2.) methanol, to room temperature
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

11-ethyl-2-methyl-5,9-dioxa-7-pentadecanone

11-ethyl-2-methyl-5,9-dioxa-7-pentadecanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 79 percent / sodium hydride / 48 h / Ambient temperature
2: PDC / dimethylformamide
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

11-ethyl-3-methyl-5,9-dioxa-7-pentadecanone

11-ethyl-3-methyl-5,9-dioxa-7-pentadecanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69 percent / sodium hydride / 48 h / Ambient temperature
2: PDC / dimethylformamide
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

11-ethyl-7-(5-methyl-2-oxa-1-hexyl)-3,6,9-trioxa-1-pentadecanol
174719-44-9

11-ethyl-7-(5-methyl-2-oxa-1-hexyl)-3,6,9-trioxa-1-pentadecanol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 79 percent / sodium hydride / 48 h / Ambient temperature
2: sodium hydride / acetonitrile / 0.5 h / Heating; before reflux 1 h room temperature
3: 1M HCl / 2 h / Heating
4: 78.7 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
5: 1.) ozone, 2.) sodium borohydride / 1.) methanol, -78 deg C, 2.) methanol, to room temperature
View Scheme
Multi-step reaction with 5 steps
1: 79 percent / sodium hydride / 48 h / Ambient temperature
2: 89 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
3: 1.) ozone, 2.) sodium borohydride / 1.) methanol, -78 deg C, 2.) methanol, to room temperature
4: 78.7 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
5: 1.) ozone, 2.) sodium borohydride / 1.) methanol, -78 deg C, 2.) methanol, to room temperature
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

11-ethyl-7-(4-methyl-2-oxa-1-hexyl)-3,6,9-trioxa-1-pentadecanol
174719-49-4

11-ethyl-7-(4-methyl-2-oxa-1-hexyl)-3,6,9-trioxa-1-pentadecanol

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 69 percent / sodium hydride / 48 h / Ambient temperature
2: 93 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
3: 1.) ozone, 2.) sodium borohydride / 1.) methanol, -78 deg C, 2.) methanol, to room temperature
4: 17 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
5: 1.) ozone, 2.) sodium borohydride / 1.) methanol, -78 deg C, 2.) methanol, to room temperature
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

9-ethyl-5-(4-methyl-2-oxa-1-hexyl)-4,7-dioxa-1-tridecene
174719-46-1

9-ethyl-5-(4-methyl-2-oxa-1-hexyl)-4,7-dioxa-1-tridecene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 69 percent / sodium hydride / 48 h / Ambient temperature
2: 93 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

9-ethyl-5-(5-methyl-2-oxa-1-hexyl)-4,7-dioxa-1-tridecene
174719-41-6

9-ethyl-5-(5-methyl-2-oxa-1-hexyl)-4,7-dioxa-1-tridecene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 79 percent / sodium hydride / 48 h / Ambient temperature
2: 89 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

12-ethyl-8-(5-methyl-2-oxa-1-hexyl)-4,7,10-trioxa-1-hexadecene
174719-43-8

12-ethyl-8-(5-methyl-2-oxa-1-hexyl)-4,7,10-trioxa-1-hexadecene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 79 percent / sodium hydride / 48 h / Ambient temperature
2: sodium hydride / acetonitrile / 0.5 h / Heating; before reflux 1 h room temperature
3: 1M HCl / 2 h / Heating
4: 78.7 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
View Scheme
Multi-step reaction with 4 steps
1: 79 percent / sodium hydride / 48 h / Ambient temperature
2: 89 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
3: 1.) ozone, 2.) sodium borohydride / 1.) methanol, -78 deg C, 2.) methanol, to room temperature
4: 78.7 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
View Scheme
2-ethyl-hexyl glycidyl ether
2461-15-6

2-ethyl-hexyl glycidyl ether

12-ethyl-8-(4-methyl-2-oxa-1-hexyl)-4,7,10-trioxa-1-hexadecene
174719-48-3

12-ethyl-8-(4-methyl-2-oxa-1-hexyl)-4,7,10-trioxa-1-hexadecene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 69 percent / sodium hydride / 48 h / Ambient temperature
2: 93 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
3: 1.) ozone, 2.) sodium borohydride / 1.) methanol, -78 deg C, 2.) methanol, to room temperature
4: 17 percent / sodium hydride / tetrahydrofuran / 22 h / 60 °C
View Scheme
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