26112-94-7Relevant academic research and scientific papers
TCT-mediated synthesis of N-acylbenzotriazoles in aqueous media
Wet-Osot, Sirawit,Phakhodee, Wong,Pattarawarapan, Mookda
, p. 6998 - 7000 (2015)
The synthesis of N-acylbenzotriazoles has been demonstrated by the 2,4,6-trichloro-1,3,5-triazine (TCT)-mediated condensation of carboxylic acids with 1H-benzotriazole in aqueous media. In saturated aqueous sodium bicarbonate, TCT was found to be relatively stable and functioned as an efficient acid activator in the acyl transfer process. This operationally simple and economic method allows the scalable synthesis of N-acylbenzotriazoles in good to excellent yields.
Facile synthesis of N-acylbenzotriazoles from carboxylic acids mediated by 2,4,6-trichloro-1,3,5-triazine and triethylamine
Wet-Osot, Sirawit,Duangkamol, Chuthamat,Pattarawarapan, Mookda,Phakhodee, Wong
, p. 959 - 963 (2015/02/19)
Abstract A facile, efficient, and economic method toward N-acylbenzotriazoles was reported using 2,4,6-trichloro-1,3,5-triazine in combination with triethylamine as a carboxylic acid activator. Through reacting 1H-benzotriazole with the generated triacylated triazine intermediate, a series of N-acylbenzotriazoles could be rapidly prepared in high yields without column chromatography.
CINNAMOYL INHIBITORS OF TRANSGLUTAMINASE
-
Page/Page column 68, (2009/01/20)
A compound of Formula, (I) or Formula: (II)
New gas-phase cascade reactions of stabilized phosphorus ylides leading to ring-fused indoles and to quinolines
Aitken, R. Alan,Murray, Lorna
supporting information; experimental part, p. 9781 - 9783 (2009/04/06)
(Chemical Equation Presented) Gas-phase cyclization processes of stabilized phosphorus ylides bearing a suitably substituted 2-aminophenyl group lead efficiently either to 3-substituted quinolines or benzo[c]-carbazole and heterocyclic-fused analogues depending on the substituents present.
