29064-02-6

Basic information

• Product Name: 8-(4-chlorophenyl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione
• Synonyms: 1H-purine-2,6-dione, 8-(4-chlorophenyl)-3,7-dihydro-1,3-dimethyl-
• CAS NO: 29064-02-6
• Molecular Formula: C₁₃H₁₁ClN₄O₂
• Molecular Weight: 290.705
• Mol File: 29064-02-6.mol
• Article Data: 8

Chemical Properties

• Boiling Point: 536.2°C at 760 mmHg
• Flash Point: 278.1°C
• Density: 1.452g/cm³
• Vapor Pressure: 1.43E-11mmHg at 25°C
• Refractive Index: 1.645
• CAS DataBase Reference: 8-(4-chlorophenyl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione(CAS DataBase Reference)
• NIST Chemistry Reference: 8-(4-chlorophenyl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione(29064-02-6)
• EPA Substance Registry System: 8-(4-chlorophenyl)-1,3-dimethyl-3,7-dihydro-1H-purine-2,6-dione(29064-02-6)

Safety Data

• Hazardous Substances Data: 29064-02-6(Hazardous Substances Data)

Upstream product

• 90994-73-3 6-(4-Chloro-benzylamino)-1,3-dimethyl-5-nitro-1H-pyrimidine-2,4-dione 
• 1203-25-4 6-chloro-1,3-dimethyl-5-nitrouracil 
• 104-86-9 4-chlorobenzylamine 
• 122-01-0 4-chloro-benzoyl chloride 
• 5440-00-6 4,5-Diamino-1,3-dimethyluracil 
• 166115-74-8 N-(6-Amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-yl)-4-chloro-benzamide 
• 42748-11-8 1,2,3,4-Tetrahydro-1,3-dimethyl-6-(4-chlorophenylmethylidenehydrazion)pyrimidin-2,4-dione 
• 13784-07-1 6-amino-5-(4-chloro-benzylideneamino)-1,3-dimethyl-1H-pyrimidine-2,4-dione 
• 147622-95-5 5-Amino-6-[(E)-1-(4-chloro-phenyl)-3-oxo-3-phenyl-propenylamino]-1,3-dimethyl-1H-pyrimidine-2,4-dione 
• 147623-04-9 8-(4-Chloro-phenyl)-1,3-dimethyl-6-phenyl-1,9-dihydro-pyrimido[4,5-b][1,4]diazepine-2,4-dione 
• 58-55-9 theophylline 
• 56075-36-6 1-(4-chlorophenyl)-2-(methylsulfonyl)diazene 

Relevant articles and documents

Smooth Metal-Free Photoinduced Preparation of Valuable 8-Arylxanthines

A set of 8-arylxanthines was prepared under metal-free conditions and in aqueous solvents from arylazo sulfones and caffeine or theophylline. Notably, the process took place by simply exposing the reaction vessel to visible or solar light, and unreacted xanthine could be easily recovered during the purification step.

REACTIONS OF 5,6-DIAMINO-1,3-DIMETYLURACIL WITH HALOGEN DERIVATIVES OF CHALCONES

The reaction of 5,6-diamino-1,3-dimethyluracil with 1,3-diaryl-2,3-dibromopropan-1-ones gave β-(5-amino-6-imino-1,3-dimethyluracil)chalcones, and conditions for their cyclocondensation to pyrimidinodiazepines were found.For substantiation of the reaction mechanism, the reaction of the diamine with other halogen derivatives of chalcones was studied.The IR, UV, and mass spectra of the synthesized compounds and their condensation products are discussed.

A NEW CONTRACTION OF PTERIDINE 5-OXIDES TO PURINES AND A 7-DEAZAPURINE BY THE 1,3-DIPOLAR CYCLOADDITION REACTION

The 1,3-dipolar cycloaddition reaction of pteridine 5-oxides with dimethyl acetylenedicarboxylate resulted in a new ring contraction of the pyrazine moiety to give purines and a 7-deazapurine.