5032-91-7Relevant academic research and scientific papers
Synthesis of 18F-radiolabeled organophosphine fluorides for thiol-chemoselective peptide conjugation
Zhuang, Huanglan,Guo, Zhide,Zhuang, Rongqiang,Zhang, Xianzhong
, p. 597 - 607 (2020/10/14)
Two 18F-radiolabeled organofluorophosphine fluorides ([18F]4 and [18F]7) for chemoselective thiol-conjugation were designed and synthesized via 18F–19F isotopic exchange reaction. This simple and rapi
Synthesis and characterization of some perfluorophenylphosphine derivatives
Magnelli,Tesi,Lowe Jr.,Mcquistion
, p. 457 - 461 (2008/10/08)
Bis(pentafluorophenyl)chlorophosphine and pentafluorophenyldichlorophosphine are prepared in good yields from pentafluorophenylmagnesium bromide and phosphorus trichloride. The reactions of the halophosphines with the Lewis bases water, ammonia, dimethylamine, and 2-methylaziridine produced substituted phosphines. Oxidative chlorination of bis(pentafluorophenyl)phosphinamide followed by dehydrohalogenation gave perfluorophenylphosphonitriles. The infrared and pertinent proton magnetic resonance spectra of these compounds are discussed.
