50483-99-3Relevant articles and documents
Method for synthesizing cyclopentyl imide
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Paragraph 0016; 0017; 0018; 0019; 0020, (2017/07/19)
The invention relates to a method for synthesizing cyclopentyl imide. The method comprises the following steps: reacting a raw material 1,2-cyclopentanediamide with an alkali liquid to generate 1,2-cyclopentanediacid, and reacting the 1,2-cyclopentanediacid with methanamide to generate the cyclopentyl imide. The synthesis method greatly reduces the cyclopentyl imide synthesis temperature to make the reaction mildly proceed, so the high temperature problem in the prior art is solved, the safety in the production process is improved, and energy saving and consumption reduction are realized; and the method has the advantages of liquid and homogenous synthesis system, stable reaction and quality, low temperature reaction conditions, no generation of coking, oxidation or carbonizing waste resides or other impurities, improvement of the quality of the above product, realization of the continuous primary yield reaching 90% or above and being about 10-30% higher than that of present technologies, stable reaction technology conditions, easiness in control, and high reaction conversion rate.
Preparation of Small Ring Carbocycles via Intramolecular Oxidative Coupling of Bisenolates Derived from α,ω-Diesters
Babler, James H.,Sarussi, Steven J.
, p. 3462 - 3464 (2007/10/02)
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Biosynthesis of brefeldin A
Handschin,Sigg,Tamm
, p. 1943 - 1965 (2007/10/05)
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