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Biphenyl 92-52-4 /manufacturer/low price/high quality/in stock
Cas No: 92-52-4
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Biphenyl CAS NO.92-52-4
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USD $ 1.0-3.0 / Kilogram 1 Kilogram 10 Kilogram/Day Hebei yanxi chemical co.,LTD. Contact Supplier
92-52-4 BIPHENYL
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92-52-4 Usage

InChI:InChI=1/C12H10/c1-3-7-11(8-4-1)12-9-5-2-6-10-12/h1-10H

92-52-4 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A10265)  Biphenyl, 99%    92-52-4 250g 242.0CNY Detail
Alfa Aesar (A10265)  Biphenyl, 99%    92-52-4 1000g 258.0CNY Detail
Alfa Aesar (A10265)  Biphenyl, 99%    92-52-4 5000g 673.0CNY Detail
Sigma-Aldrich (96996)  Biphenyl  certified reference material, TraceCERT® 92-52-4 96996-100MG 1,054.17CNY Detail
Supelco (442487)  Biphenyl  analytical standard 92-52-4 000000000000442487 362.70CNY Detail
Sigma-Aldrich (35800)  Biphenyl  PESTANAL®, analytical standard 92-52-4 35800-1G 188.37CNY Detail
Supelco (48161)  Biphenylsolution  certified reference material, 2000 μg/mL in methanol 92-52-4 000000000000048161 362.70CNY Detail
USP (1073423)  Biphenyl  United States Pharmacopeia (USP) Reference Standard 92-52-4 1073423-500MG 4,647.24CNY Detail

92-52-4SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 16, 2017

Revision Date: Aug 16, 2017

1.Identification

1.1 GHS Product identifier

Product name biphenyl

1.2 Other means of identification

Product number -
Other names 1,1‘-Biphenyl

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only. Biphenyl is used in organic syntheses, heat transfer fluids, dye carriers, food preservatives, as an intermediate for polychlorinated biphenyls, and as a fungistat in the packaging of citrus fruits.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:92-52-4 SDS

92-52-4Synthetic route

dibenzothiophene
132-65-0

dibenzothiophene

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With Ni-MoS2 supported on γ-Al2O3 at 320℃; Temperature; Reagent/catalyst;100%
With 3-Hydroxy-1-methylpiperidine; nickel diacetate; sodium hydride In tetrahydrofuran at 65℃; for 1.25h;95%
With lithium aluminium tetrahydride; (2,2'-bipyridyl)(1,5-cyclooctadiene)nickel In tetrahydrofuran at 55 - 60℃; for 48h; Product distribution; further reagent ratio;90%
bromobenzene
108-86-1

bromobenzene

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With palladium diacetate; triethylamine; 2-diphenylphosphino-2'-methylbiphenyl In N,N-dimethyl-formamide at 100℃; for 5h; Ullmann reaction; Inert atmosphere;100%
With potassium carbonate In ethanol; water at 20℃; for 12h; Ullmann Condensation;100%
dibromobis(triphenylphosphine)nickel(II); tetraethylammonium iodide; zinc In tetrahydrofuran at 50℃; for 1.5h;99%
iodobenzene
591-50-4

iodobenzene

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With [Pd{C6H4(CH2N(CH2Ph)2)}(μ-Br)]2; potassium carbonate In 1-methyl-pyrrolidin-2-one at 130℃; for 2h; Microwave irradiation;100%
With sodium tetraphenyl borate; sodium carbonate In 1-methyl-pyrrolidin-2-one at 130℃; for 4h; Suzuki coupling; Inert atmosphere;99%
With potassium carbonate In ethanol; water at 80℃; for 4h; Reagent/catalyst; Solvent; Ullmann Condensation; Green chemistry;99.2%
m-chlorobiphenyl
2051-61-8

m-chlorobiphenyl

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With water In ethanol for 30h; Irradiation; Sealed tube; Inert atmosphere;100%
With water; potassium formate at 100℃; for 24h; Inert atmosphere;91%
With sodium hydroxide; Raney Ni-Al alloy In water at 60℃; for 2h; Irradiation;83%
4-bromo-1,1'-biphenyl
92-66-0

4-bromo-1,1'-biphenyl

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With hydrogen In methanol at 20℃; for 24h;100%
Stage #1: 4-bromo-1,1'-biphenyl With n-butyllithium In tetrahydrofuran at -50℃; for 0.5h;
Stage #2: With phenylacetonitrile In tetrahydrofuran at -50 - 20℃; for 0.5h; Further stages;
99%
With [RhCl2(p-cymene)]2; potassium tert-butylate In isopropyl alcohol at 20 - 100℃; for 24h; Inert atmosphere;97%
phenylmagnesium bromide
100-58-3

phenylmagnesium bromide

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With 3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone at -20℃; Product distribution / selectivity;100%
With iron(III) chloride; 1,2-dichloro-ethane In tetrahydrofuran at 0℃; for 0.0833333h; Ionic liquid; Inert atmosphere;100%
With 1,2-bisperfluorotolyl-3,3,4,4,5,5-hexafluorocyclopentene In tetrahydrofuran at 25℃; for 1h; Reagent/catalyst; Inert atmosphere;99%
triphenylbismuthane
603-33-8

triphenylbismuthane

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With triethylamine; palladium diacetate In N,N,N,N,N,N-hexamethylphosphoric triamide at 65℃; for 0.166667h;100%
With para-bromotoluene; C22H25ClNPPdS; potassium carbonate In 1,4-dioxane at 100℃; for 6h; Inert atmosphere; Schlenk technique;48%
With 2-thioxo-3H-1,3-benzothiazole; copper diacetate; bis(dibenzylideneacetone)-palladium(0) In 1,2-dichloro-ethane at 80℃; for 24h; Inert atmosphere;19 %Chromat.
triphenyl bismuth (2+); dichloride
507233-69-4, 594-30-9, 28719-54-2

triphenyl bismuth (2+); dichloride

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With triethylamine; palladium diacetate In tetrahydrofuran for 0.5h; Ambient temperature;100%
chlorobenzene
108-90-7

chlorobenzene

phenylmagnesium bromide
100-58-3

phenylmagnesium bromide

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
nickel(II) In tetrahydrofuran for 18h; Product distribution; other catalyst, other solvents; other Grignard compounds and alkyl or vinyl halides;100%
With CpNi[1-(ethoxycarbonyl)methyl-3-(3,5-dimethylbenzyl)benzimidazolin-2-ylidene]Br In tetrahydrofuran at 25℃; for 3h; Kumada Cross-Coupling; Inert atmosphere; Schlenk technique;97%
With Pd/Al(OH)3 In toluene at 140℃; for 36h; Kumada Cross-Coupling; Inert atmosphere;94%
chlorobenzene
108-90-7

chlorobenzene

phenylboronic acid
98-80-6

phenylboronic acid

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With Cs2O3; PCy3 adduct of cyclopalladated ferrocenylimine In 1,4-dioxane at 100℃; for 15h; Suzuki cross-coupling reaction;100%
With dichloro(cycloocta-1,5-diene)palladium (II); 2,2-[μ-(N,N'-piperazindiyl)dimethyl]-bis(4,6-di-tert-butyl-phenol); potassium carbonate In methanol for 0.166667h; Suzuki cross-coupling reaction; Microwave irradiation; Inert atmosphere;100%
With potassium carbonate In methanol at 100℃; for 0.0833333h; Suzuki-Miyaura Coupling; Microwave irradiation;100%
4'-biphenyl chloride
2051-62-9

4'-biphenyl chloride

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With sodium tetrahydroborate; 2-methoxy-ethanol; nickel dichloride In tetrahydrofuran at 68℃; for 1.25h; Product distribution; other dechlorinating agents and times;100%
With potassium hydroxide; Cp*Rh(OAc)2*H2O In various solvent(s) for 17h; Heating;100%
With sodium tetrahydroborate; lithium chloride In diethylene glycol dimethyl ether r.t., 30 min then 130 deg C, 10 min;99%
bromobenzene
108-86-1

bromobenzene

phenylboronic acid
98-80-6

phenylboronic acid

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With potassium carbonate; {1,3-di[(R)-1-PhEt]imidazolin-2-ylidene}(PPh3)PdI2 In xylene at 130℃; for 13h; Suzuki-Miyaura cross-coupling reaction;100%
With potassium phosphate; triphenylphosphine; Ni(II) complexes of bidentate carbene; phosphine ligand In toluene at 80℃; Suzuki cross-coupling;100%
With [PdCl2(2-ethyl-2-oxazoline)2]; potassium carbonate In toluene at 110℃; for 3h; Suzuki reaction;100%
iodobenzene
591-50-4

iodobenzene

phenylboronic acid
98-80-6

phenylboronic acid

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With potassium carbonate; copper-palladium In N,N-dimethyl-formamide at 110℃; Kinetics; Product distribution; Further Variations:; Catalysts; Reaction partners; Suzuki cross-coupling;100%
With sodium hydroxide; Pd-dodecanethiolate nanoparticles In tetrahydrofuran at 20℃; for 24h; Suzuki-Miyaura cross-coupling;100%
With sodium carbonate; 1-butyl-3-methylimidazolium Tetrafluoroborate; 2C10H15N2(1+)*Cl4Pd(2-) In water at 110℃; for 12h; Conversion of starting material; Suzuki Coupling;100%
2-Bromobiphenyl
2052-07-5

2-Bromobiphenyl

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With LiCrH4*2LiCl*2THF In tetrahydrofuran at 25℃;100%
With vanadium monochloride In tetrahydrofuran at 25℃; for 12h; Inert atmosphere;100%
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; potassium tert-butylate; isopropyl alcohol at 100℃; Schlenk technique; Inert atmosphere;96%
4-iodo-biphenyl
1591-31-7

4-iodo-biphenyl

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With LiCrH4*2LiCl*2THF In tetrahydrofuran at 25℃; for 12h;100%
With potassium tert-butylate; benzyl alcohol In N,N-dimethyl-formamide at 90℃; for 2h; Reagent/catalyst; Solvent; Schlenk technique; Inert atmosphere;98%
With potassium tert-butylate; benzaldehyde In N,N-dimethyl-formamide at 90℃; for 2h; Schlenk technique; Inert atmosphere;96%
phenylboronic acid
98-80-6

phenylboronic acid

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With Tetradecanoic acid 1-methylethyl ester; palladium diacetate; potassium carbonate In water at 20℃; for 0.25h; Catalytic behavior; Reagent/catalyst; Green chemistry;100%
With bis[1-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)-3-methyl-4-phenyl-1,2,3-triazol-5-ylidene]palladium(II) iodide; potassium tert-butylate; chlorobenzene In ethanol at 20℃; for 2h; Reagent/catalyst; Inert atmosphere;100%
With Triphenylmethylamin; potassium carbonate; 4-chlorobenzonitrile; palladium dichloride In water at 20℃; for 24h;99%
Perbenzoic acid
93-59-4

Perbenzoic acid

bis-benzenesulfenyl-amine
24364-84-9

bis-benzenesulfenyl-amine

A

benzoic acid phenyl ester
93-99-2

benzoic acid phenyl ester

B

biphenyl
92-52-4

biphenyl

C

benzoic acid
65-85-0

benzoic acid

D

diphenyldisulfane
882-33-7

diphenyldisulfane

E

N2, tar

N2, tar

Conditions
ConditionsYield
In benzene Kinetics; Product distribution; Mechanism; isotopic effect, effect of benzoic acid and styrene on the reaction;A 1.4%
B 0.2%
C 100%
D 50%
E n/a
iodobenzene
591-50-4

iodobenzene

tetra-n-butylammonium phenyltrifluoroborate

tetra-n-butylammonium phenyltrifluoroborate

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With caesium carbonate; 1,4-di(diphenylphosphino)-butane; palladium diacetate In 1,2-dimethoxyethane; water at 20℃; for 12h;100%
iodobenzene
591-50-4

iodobenzene

dichloromethylphenylsilane
149-74-6

dichloromethylphenylsilane

biphenyl
92-52-4

biphenyl

Conditions
ConditionsYield
With potassium hydroxide; palladium on activated charcoal In water at 100℃;100%
With potassium hydroxide; palladium on activated charcoal In water Heating;100%
1-bromo-4-methoxy-benzene
104-92-7

1-bromo-4-methoxy-benzene

phenylboronic acid
98-80-6

phenylboronic acid

A

biphenyl
92-52-4

biphenyl

B

4-methoxylbiphenyl
613-37-6

4-methoxylbiphenyl

Conditions
ConditionsYield
With potassium hydroxide In toluene at 100℃; for 6h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique;A n/a
B 100%
With C34H28Cl2N2P2Pd(2+); potassium carbonate In isopropyl alcohol at 20℃; for 4h; Reagent/catalyst; Suzuki-Miyaura Coupling;A 3%
B 98%
With potassium carbonate In ethanol; water at 60℃; for 5h; Catalytic behavior; Suzuki-Miyaura Coupling;A 6.3%
B 87%
para-nitrophenyl bromide
586-78-7

para-nitrophenyl bromide

phenylboronic acid
98-80-6

phenylboronic acid

A

biphenyl
92-52-4

biphenyl

B

1-phenyl-4-nitrobenzene
92-93-3

1-phenyl-4-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In ethanol; water at 60℃; for 5h; Catalytic behavior; Suzuki-Miyaura Coupling;A 11%
B 100%
With potassium tert-butylate; tetrabutylammomium bromide; palladium diacetate In tetrahydrofuran; water at 50℃; for 24h; Suzuki-type cross-coupling reaction;A 1%
B 99%
With Triphenylmethylamin; potassium carbonate; palladium dichloride In water at 20℃; for 20h; Suzuki-Miyaura reaction;A 6%
B 98%
With potassium carbonate; copper-palladium In N,N-dimethyl-formamide at 110℃; for 0.5h; Kinetics; Product distribution; Further Variations:; Reaction partners; Suzuki cross-coupling;A n/a
B 95.5%
diphenyliodonium bromide
1483-73-4

diphenyliodonium bromide

mercury

mercury

A

iodobenzene
591-50-4

iodobenzene

B

biphenyl
92-52-4

biphenyl

C

mercury(I) bromide

mercury(I) bromide

D

bromo(phenyl)mercury
1192-89-8

bromo(phenyl)mercury

E

benzene
71-43-2

benzene

Conditions
ConditionsYield
In acetonitrile Kinetics; byproducts: C6H5Br; at different temp. between 20-70°C; UV; yields for 45°C;A 100%
B 6-7
C n/a
D n/a
E 1.4%
diphenyliodonium chloride
1483-72-3

diphenyliodonium chloride

mercury

mercury

A

iodobenzene
591-50-4

iodobenzene

B

mercury(I) chloride

mercury(I) chloride

C

biphenyl
92-52-4

biphenyl

D

phenylmercury(II) chloride
100-56-1

phenylmercury(II) chloride

E

benzene
71-43-2

benzene

Conditions
ConditionsYield
In acetonitrile Kinetics; at different temp. between 20-70°C; UV; yields for 45°C;A 100%
B 10-11
C 4-5
D 89-92
E 1.4%
bromobenzene
108-86-1

bromobenzene

phenylboronic acid
98-80-6

phenylboronic acid

A

biphenyl
92-52-4

biphenyl

B

bromoboronate
146175-56-6

bromoboronate

Conditions
ConditionsYield
With K2CO3; diiodo(1,3-di[(R)-1-phenylethyl]imidazolin-2-ylidene)(triphenylphosphino)palladium(II) In xylene the mixt. in xylene was heated at 130°C for 13 h (N2); H2O was added, the aq. phase was extd. with diethyl ether, the organic phase was dried over MgSO4;A 100%
B n/a
phenylzinc chloride
28557-00-8

phenylzinc chloride

allyl bromide
106-95-6

allyl bromide

A

allylbenzene
300-57-2

allylbenzene

B

biphenyl
92-52-4

biphenyl

C

zinc dibromide

zinc dibromide

Conditions
ConditionsYield
tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran Ar atmosphere; stirring (20°C, 5 mole-% catalyst, 3.5 h);A 100%
B 0%
C n/a
bis(η3-allyl-μ-chloropalladium(II)) In tetrahydrofuran Ar atmosphere; stirring (20°C, 5 mole-% catalyst, 3 h);A 55%
B 40%
C n/a
Allyl acetate
591-87-7

Allyl acetate

phenylzinc chloride
28557-00-8

phenylzinc chloride

A

allylbenzene
300-57-2

allylbenzene

B

biphenyl
92-52-4

biphenyl

C

zinc diacetate
557-34-6

zinc diacetate

Conditions
ConditionsYield
tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran Ar atmosphere; stirring (20°C, 5 mole-% catalyst, 5 h);A 100%
B 0%
C n/a
triphenylphosphinediiodogermylene
97939-92-9

triphenylphosphinediiodogermylene

phenyllithium
591-51-5

phenyllithium

A

iodobenzene
591-50-4

iodobenzene

B

biphenyl
92-52-4

biphenyl

C

triphenylgermane
2816-43-5

triphenylgermane

D

tetraphenylgermane
1048-05-1

tetraphenylgermane

E

triphenylphosphine
603-35-0

triphenylphosphine

Conditions
ConditionsYield
In diethyl ether under N2, to suspn. of Ph3PGeI2 in ether PhLi added dropwise (1:4 molarratio), stirred for 5 d under reflux, hydrolyzed; dried, analyzed by gas chromy.;A 10%
B 13%
C 39%
D 36%
E 100%
In diethyl ether under N2, to suspn. of Ph3PGeI2 in ether PhLi added dropwise (1:1 molarratio), stirred for 5 d under reflux, hydrolyzed; dried, analyzed by gas chromy.;A 2.9%
B 2.9%
C 1.9%
D 14%
E 82%
In diethyl ether under N2, to suspn. of Ph3PGeI2 in ether PhLi added dropwise (1:2 molarratio), stirred for 5 d under reflux, hydrolyzed; dried, analyzed by gas chromy.;A 7.7%
B 9.6%
C 1.3%
D 19%
E 79%
(2E)-ethyl 3-chloro-2-iodobut-2-enoate
888039-38-1

(2E)-ethyl 3-chloro-2-iodobut-2-enoate

phenylboronic acid
98-80-6

phenylboronic acid

A

biphenyl
92-52-4

biphenyl

B

ethyl (E)-3-phenylbut-2-enoate
945-93-7, 13979-22-1, 1504-72-9

ethyl (E)-3-phenylbut-2-enoate

Conditions
ConditionsYield
With caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate; tris(dibenzylideneacetone)dipalladium (0) In 1,4-dioxane for 4h; Heating;A 100%
B 99%
bromobenzene
108-86-1

bromobenzene

methyl (L)-leucinate hydrochloride
7517-19-3

methyl (L)-leucinate hydrochloride

A

biphenyl
92-52-4

biphenyl

B

(S)-2-amino-1,1-diphenyl-4-methylpentan-1-ol
78603-97-1

(S)-2-amino-1,1-diphenyl-4-methylpentan-1-ol

Conditions
ConditionsYield
Stage #1: bromobenzene With magnesium In diethyl ether at 40℃; Inert atmosphere;
Stage #2: methyl (L)-leucinate hydrochloride In diethyl ether at 0 - 20℃; for 15.5h;
A n/a
B 100%
biphenyl
92-52-4

biphenyl

3-phenyl-1,4-cyclohexadiene
4794-05-2

3-phenyl-1,4-cyclohexadiene

Conditions
ConditionsYield
With ammonia; lithium In diethyl ether; water at -78 - -25℃; for 0.5h;100%
With ammonia; lithium In diethyl ether for 0.416667h;92%
With ammonia; sodium In diethyl ether at -78℃; Birch Reduction;50%
biphenyl
92-52-4

biphenyl

4,4'-diiodobiphenyl
3001-15-8

4,4'-diiodobiphenyl

Conditions
ConditionsYield
With sulfuric acid; iodine; periodic acid; acetic acid In tetrachloromethane at 80℃; for 4h;100%
With iodine; bis-[(trifluoroacetoxy)iodo]benzene In tetrachloromethane for 0.25h; Ambient temperature;87%
With iodine; bis-[(trifluoroacetoxy)iodo]benzene In tetrachloromethane for 0.25h; Ambient temperature;87%
biphenyl
92-52-4

biphenyl

isobutyryl chloride
79-30-1

isobutyryl chloride

1-([1,1′-biphenyl]-4-yl)-2-methylpropan-1-one
6976-20-1

1-([1,1′-biphenyl]-4-yl)-2-methylpropan-1-one

Conditions
ConditionsYield
With aluminium trichloride In dichloromethane at 0 - 20℃; for 14.5h;100%
With aluminium trichloride In carbon disulfide Friedel-Crafts acylation; Heating;54%
With carbon disulfide; aluminium trichloride
With aluminium trichloride In carbon disulfide
With aluminum (III) chloride In 1,2-dichloro-ethane at 5 - 10℃; for 5h; Solvent; Temperature;
biphenyl
92-52-4

biphenyl

tertiary butyl chloride
507-20-0

tertiary butyl chloride

4,4'-di-tert-butylbiphenyl
1625-91-8

4,4'-di-tert-butylbiphenyl

Conditions
ConditionsYield
iron(III) chloride In dichloromethane at 20℃;100%
With iron(III) chloride In dichloromethane100%
With iron(III) chloride In dichloromethane at 22 - 40℃;97%
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