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Name	1,10-Phenanthroline monohydrochloride	EINECS	223-325-1
CAS No.	3829-86-5	Density	1.385 g/cm3 (-100.15 C)
PSA	25.78000	LogP	3.58500
Solubility	soluble in water	Melting Point	224-225 °C(lit.)
Formula	C₁₂H₈N₂^.HCl	Boiling Point	365.1 °C at 760 mmHg
Molecular Weight	216.67	Flash Point	164.8 °C
Transport Information	UN 2811 6.1/PG 3	Appearance	white to light yellow or slightly purple powder
Safety	45-60-61	Risk Codes	25-50/53
Molecular Structure		Hazard Symbols	T, N
Synonyms	1,10-Phenanthroline,monohydrochloride (8CI,9CI);1,10-Diazaphenanthrene hydrochloride;1,10-Phenanthroline hydrochloride;NSC 4265;

1,10-Phenanthroline monohydrochloride Synthetic route

: 3829-86-5
1,10-phenanthroline hydrochloride

: copper dichloride

: (1,5,9,13-tetraaza-3,4,7,8,11,12,15,16-tetrabenzocyclohexadeca-1,3,5,7,9,11,13,16-octaene)copper(I) nitrate

Conditions

Conditions	Yield
In water from aq. soln. of CuCl2 and soln. of phenanthroline hydrochloride in 2:1, 1:1 molar ratio at pH 6.5 maintained by an alkali soln.; solvent evapd. in a water bath; ppt. washed (H2O); dried (air); elem. anal.;	96%

: 3829-86-5
1,10-phenanthroline hydrochloride

: copper dichloride

: [Cu(II)(1,10-phenantroline)2(H2O)]Cl2 complex

Conditions

Conditions	Yield
In water from aq. soln. of CuCl2 and soln. of phenanthroline hydrochloride in 1:2, 1:3 molar ratio at pH 6.5 maintained by an alkali soln.; solvent evapd. in a water bath; ppt. washed (H2O); dried (air); elem. anal.;	90%

: 3829-86-5
1,10-phenanthroline hydrochloride

: 90076-65-6
bis(trifluoromethane)sulfonimide lithium

: 1309962-26-2
C2HF6NO4S2*C12H8N2

Conditions

Conditions	Yield
With water at 20℃; for 2h;	90%

: copper(II) choride dihydrate

: 3829-86-5
1,10-phenanthroline hydrochloride

: 555-06-6
sodium p-aminobenzoate

: [Cu(phen)2Cl]Cl*2p‑aminobenzoic acid*4H2O

Conditions

Conditions	Yield
In methanol for 1h;	88%

: 7722-64-7
potassium permanganate

: ammonium chloride

: 7732-18-5
water

: 3829-86-5
1,10-phenanthroline hydrochloride

: 12775-96-1, 15158-11-9, 15721-63-8, 16941-75-6, 17493-86-6, 19498-52-3, 20499-83-6, 20499-84-7, 20499-85-8, 20499-86-9, 20573-10-8, 20573-11-9, 21595-51-7, 21595-52-8, 22206-52-6, 26445-28-3, 28959-95-7, 37362-93-9, 39417-05-5, 54603-16-6, 54603-23-5, 54603-32-6, 54603-40-6, 54603-48-4, 54603-81-5, 54603-89-3, 56316-56-4, 95985-91-4, 122297-32-9, 7440-50-8
copper

: [Cu(1,10-phenanthroline)2Cl]2[MnCl3(1,10-phenanthroline)]Cl*2water

Conditions

Conditions	Yield
In methanol byproducts: Mn(2+); stirring 1:1:2:2 mixt. of copper, permanganate salt, phenanthroline deriv., NH4Cl in methanol at 50-60°C in air for 2 h; addn. of isopropanol, isolation of crystals, elem. anal.;	87%

...Expand

: 7722-64-7
potassium permanganate

: ammonium chloride

: 3829-86-5
1,10-phenanthroline hydrochloride

: 12775-96-1, 15158-11-9, 15721-63-8, 16941-75-6, 17493-86-6, 19498-52-3, 20499-83-6, 20499-84-7, 20499-85-8, 20499-86-9, 20573-10-8, 20573-11-9, 21595-51-7, 21595-52-8, 22206-52-6, 26445-28-3, 28959-95-7, 37362-93-9, 39417-05-5, 54603-16-6, 54603-23-5, 54603-32-6, 54603-40-6, 54603-48-4, 54603-81-5, 54603-89-3, 56316-56-4, 95985-91-4, 122297-32-9, 7440-50-8
copper

: 68-12-2, 33513-42-7
N,N-dimethyl-formamide

: [Cu(1,10-phenanthroline)2Cl]2[MnCl4]*DMF

Conditions

Conditions	Yield
In methanol; N,N-dimethyl-formamide byproducts: Mn(2+); stirring 1:1:2:2 mixt. of copper, permanganate salt, phenanthroline deriv., NH4Cl in methanol and DMF at 50-60°C in air for 2 h; addn. of isopropanol, isolation of crystals, elem. anal.;	82%

...Expand

: HP(C2H5)2C6H5(1+)*Cr(NCS)4(P(C2H5)2C6H5)2(1-) = {HP(C2H5)2C6H5}{Cr(NCS)4(P(C2H5)2C6H5)2}

: 3829-86-5
1,10-phenanthroline hydrochloride

: C12H9N2(1+)*Cr(NCS)4(P(C2H5)2C6H5)2(1-) = {C12H9N2}{Cr(NCS)4(P(C2H5)2C6H5)2}

Conditions

Conditions	Yield
In methanol; water; butan-1-ol dissolving of amine hydrochloride in water, addn. of the phosphine-complex in methanol-butanol; filtn. after 10-15 min, washing (methanol), drying at room temp. in air, elem. anal.;	72%

: nitridotechnetic(VI) acid

: 3829-86-5
1,10-phenanthroline hydrochloride

: 131810-72-5
nitridoperoxo 1,10-phenanthroline technetium(VII)

Conditions

Conditions	Yield
elem. anal.;	70%

: {HP(C2H5)2C6H4CH3}(1+)*Cr(NCS)4(P(C2H5)2C6H4CH3)2(1-) = {HP(C2H5)2C6H4CH3}{Cr(NCS)4(P(C2H5)2C6H4CH3)2}

: 3829-86-5
1,10-phenanthroline hydrochloride

: C12H9N2(1+)*Cr(NCS)4(P(C2H5)2C6H4CH3)2(1-) = {C12H9N2}{Cr(NCS)4(P(C2H5)2C6H4CH3)2}

Conditions

Conditions	Yield
In water dissolving of amine hydrochloride in water, addn. of Cr complex; addn. of methanol-butanol, filtn. after 10-15 min, washing (methanol), drying at room temp. in air, elem. anal.;	65%

: mer-diaqua(oxydiacetato)oxovanadium(IV)

: 3829-86-5
1,10-phenanthroline hydrochloride

: o-phenanthroline(oxydiacetato)oxovanadium(IV) monohydrate

Conditions

Conditions	Yield
In water under anaerobic conditions; water soln. of ligand (1 equiv.) added slowly to aq. soln. of V complex; left to stand for 4 d; crystals collected; elem. anal.;	53%

1,10-Phenanthroline monohydrochloride Chemical Properties

The Molecular Structure of 1,10-Phenanthroline, hydrochloride (1:1) (CAS NO.3829-86-5):

Empirical Formula: C₁₂H₉ClN₂
Molecular Weight: 216.6663
IUPAC: 1,10-phenanthroline hydrochloride
Nominal Mass: 216 Da
Average Mass: 216.6663 Da
Monoisotopic Mass: 216.045426 Da
Flash Point: 164.8 °C
Enthalpy of Vaporization: 58.73 kJ/mol
Boiling Point: 365.1 °C at 760 mmHg
Melting Point: 224-225 °C(lit.)
Solubility H2O: 0.1 g/mL, clear
Water Solubility: soluble
BRN: 4007967
Appearance: white to light yellow or slightly purple powder
Vapour Pressure: 3.38E-05 mmHg at 25°C
InChI
InChI=1/C12H8N2.ClH/c1-3-9-5-6-10-4-2-8-14-12(10)11(9)13-7-1;/h1-8H;1H
Smiles
c12c3ncccc3ccc2cccn1.Cl
Product Categories: Aromatic Hydrocarbons (substituted) & Derivatives;Heterocyclic Compounds;Analytical Chemistry;Chelating Reagents;Phenanthrolines

1,10-Phenanthroline monohydrochloride Safety Profile

Hazard Codes: Toxic T Dangerous N
Risk Statements: 25-50/53
R25 :Toxic if swallowed
R50/53:Very toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment
Safety Statements: 45-60-61
S45:In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
S60:This material and its container must be disposed of as hazardous waste
S61:Avoid release to the environment. Refer to special instructions / safety data sheets
RIDADR UN: 2811 6.1/PG 3
WGK Germany: 3
F 8:Photosensitive
HazardClass: 6.1
PackingGroup :III

1,10-Phenanthroline monohydrochloride Specification

1,10-Phenanthroline, hydrochloride (1:1) (CAS NO.3829-86-5) is also called as 1,10-Diazaphenanthrene hydrochloride ; 1,10-Phenanthroline hydrochloride ; EINECS 223-325-1 ; NSC 4265 ; Phenanthroline hydrochloride ; 1,10-Phenanthroline monohydrochloride monohydrate ; 1,10-Phenanthroline, monohydrochloride .

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