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Cas Database |
| Name |
1,5-Diazocine, octahydro |
EINECS | N/A |
| CAS No. | 5687-07-0 | Density | 0.852 |
| PSA | 24.06000 | LogP | 0.61700 |
| Solubility | N/A | Melting Point |
N/A |
| Formula | C6H14 N2 | Boiling Point | 194ºC |
| Molecular Weight | 114.191 | Flash Point | 84ºC |
| Transport Information | N/A | Appearance | N/A |
| Safety | Risk Codes | N/A | |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
(1,5)Diazocane;1,5-Diazacyclooctane; Octahydro-1,5-diazocine |
Article Data | 15 |
1,5-Diazocine, octahydro Synthetic route
- 40422-46-6
1,5-diazabicyclooctane dihydrobromide
- 5687-07-0
1,5-diazacyclooctane
Conditions
| Conditions | Yield |
|---|---|
| With sodium methylate In methanol at 70℃; for 0.166667h; | 98% |
- 67761-04-0
1,5-bis(p-toluenesulphonyl)-1,5-diazacyclooctane
- 5687-07-0
1,5-diazacyclooctane
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen bromide; phenol at 80℃; for 60h; | 86% |
Conditions
| Conditions | Yield |
|---|---|
| at 120℃; im Rohr; |
Conditions
| Conditions | Yield |
|---|---|
| With water; nickel Hydrogenation; | |
| With diisobutylaluminum hydride |
- 35513-93-0
N1-(cyanoethyl)-1,3-propanediamine
- 5687-07-0
1,5-diazacyclooctane
Conditions
| Conditions | Yield |
|---|---|
| With sodium; butan-1-ol |
Conditions
| Conditions | Yield |
|---|---|
| With tetrafluoroboric acid for 0.5h; Product distribution; Heating; t1/2; further reagent:NaOH/D2O; |
- 5687-07-0
1,5-diazacyclooctane
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride at 180℃; |
- 64-17-5
ethanol
- 142-28-9
1,3-Dichloropropane
- 302-01-2
hydrazine
A
- 504-70-1
pyrazolidine
B
- 5687-07-0
1,5-diazacyclooctane
...Expand
- 75321-10-7
3-propyl tosylate
- 5687-07-0
1,5-diazacyclooctane
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 1.) sodium hydride / 1.) DMF, 80 deg C, 2.5 h, 2.) DMF, 80 deg C, 24 h 2: 86 percent / phenol, 33percent HBr in acetic acid / 60 h / 80 °C View Scheme |
- 56187-12-3
N-tosyl-bis(3-hydroxypropyl)amine
- 5687-07-0
1,5-diazacyclooctane
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: 65 percent / triethylamine, 4-dimethylaminopyridine (DMAP) / CH2Cl2 / 2 h / Ambient temperature 2: 1.) sodium hydride / 1.) DMF, 80 deg C, 2.5 h, 2.) DMF, 80 deg C, 24 h 3: 86 percent / phenol, 33percent HBr in acetic acid / 60 h / 80 °C View Scheme |
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1,5-DIAZACYCLOOCTANE
