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Cas Database |
| Name |
2-Chlorofluorene |
EINECS | N/A |
| CAS No. | 2523-44-6 | Density | 1.251 g/cm3 |
| PSA | 0.00000 | LogP | 3.91120 |
| Solubility | N/A | Melting Point |
96-97°C |
| Formula | C13H9 Cl | Boiling Point | 333.4 °C at 760 mmHg |
| Molecular Weight | 200.667 | Flash Point | 157.5 °C |
| Transport Information | N/A | Appearance | white crystal |
| Safety | Risk Codes | N/A | |
| Molecular Structure |
|
Hazard Symbols | N/A |
| Synonyms |
Fluorene,2-chloro- (6CI,7CI,8CI); 2-Chlorofluorene; NSC 97412 |
Article Data | 30 |
2-Chlorofluorene Synthetic route
- 2523-44-6
2-chloro-9H-fluorene
| Conditions | Yield |
|---|---|
| With bis-triphenylphosphine-palladium(II) chloride; caesium carbonate; Trimethylacetic acid In tetrahydrofuran at 25℃; for 18h; Glovebox; Schlenk technique; Inert atmosphere; | 99% |
- 2523-44-6
2-chloro-9H-fluorene
| Conditions | Yield |
|---|---|
| With [bis(acetoxy)iodo]benzene; (R)-10-camphorsulfonic acid; tetrahydrothiophene gold(III) bromide In methanol; chloroform at 27℃; for 3h; Schlenk technique; Inert atmosphere; | 90% |
- 179526-95-5
2-bromo-4,4’-dichloro-1,1’-biphenyl
- 18107-18-1
diazomethyl-trimethyl-silane
- 2523-44-6
2-chloro-9H-fluorene
| Conditions | Yield |
|---|---|
| With tetrakis(triphenylphosphine) palladium(0); potassium acetate; potassium carbonate In 1,4-dioxane at 100℃; for 24h; Inert atmosphere; | 90% |
| Conditions | Yield |
|---|---|
| With potassium acetate; palladium diacetate; potassium hydrogencarbonate; isopropyl alcohol In N,N-dimethyl acetamide; water; N,N-dimethyl-formamide at 75℃; for 10h; Schlenk technique; Inert atmosphere; | 84% |
- 2523-44-6
2-chloro-9H-fluorene
| Conditions | Yield |
|---|---|
| With trifluoroacetic acid In toluene at 100℃; for 1h; | 75% |
| Conditions | Yield |
|---|---|
| With potassium acetate; palladium diacetate; potassium hydrogencarbonate; isopropyl alcohol In N,N-dimethyl acetamide; water; N,N-dimethyl-formamide at 75℃; for 10h; Schlenk technique; Inert atmosphere; | 64% |
| Conditions | Yield |
|---|---|
| at 0 - 5℃; |
2-Chlorofluorene Chemical Properties
Molecular Structure:
Molecular Formula: C13H9Cl
Molecular Weight: 200.6636
IUPAC Name: 2-Chloro-9H-fluorene
Synonyms of 2-Chlorofluorene (CAS NO.2523-44-6): AI3-01713 ; NSC 97412 ; 9H-Fluorene, 2-chloro- (9CI) ; Fluorene, 2-chloro- (8CI)
CAS NO: 2523-44-6
Product Categories: Electronic Chemicals
Melting point: 96-97°C
Index of Refraction: 1.653
Molar Refractivity: 58.69 cm3
Molar Volume: 160.2 cm3
Surface Tension: 48.3 dyne/cm
Density: 1.251 g/cm3
Flash Point: 157.5 °C
Enthalpy of Vaporization: 55.34 kJ/mol
Boiling Point: 333.4 °C at 760 mmHg
Vapour Pressure of 2-Chlorofluorene (CAS NO.2523-44-6): 0.000265 mmHg at 25°C
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