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Cas Database

Name	3-Methoxy-4-methylbenzaldehyde	EINECS	N/A
CAS No.	24973-22-6	Density	1.062 g/cm³
PSA	26.30000	LogP	1.81610
Solubility	N/A	Melting Point	40.5-41.5 °C
Formula	C₉H₁₀O₂	Boiling Point	246.2 °C at 760 mmHg
Molecular Weight	150.177	Flash Point	105.7 °C
Transport Information	N/A	Appearance	N/A
Safety	26-36/37/39	Risk Codes	36/37/38
Molecular Structure		Hazard Symbols	Xi
Synonyms	m-Anisaldehyde,4-methyl- (7CI,8CI);3-Methoxy-p-tolualdehyde;	Article Data	23

3-Methoxy-4-methylbenzaldehyde Synthetic route

: 4685-50-1
3-methoxy-4-methylbenzyl alcohol

: 24973-22-6
3-methoxy-4-methylbenzaldehyde

Conditions

Conditions	Yield
With Dess-Martin periodane In dichloromethane at 0℃; for 0.5h;	100%
With manganese(IV) oxide In tetrahydrofuran for 2h;	95%
With manganese(IV) oxide In dichloromethane for 2h; Heating;	90%

: 57295-30-4
3-hydroxy-4-methylbenzaldehyde

: 77-78-1
dimethyl sulfate

: 24973-22-6
3-methoxy-4-methylbenzaldehyde

Conditions

Conditions	Yield
With potassium hydroxide at 45℃;	91%
With potassium hydroxide	87%

: 57295-30-4
3-hydroxy-4-methylbenzaldehyde

: 74-88-4
methyl iodide

: 24973-22-6
3-methoxy-4-methylbenzaldehyde

Conditions

Conditions	Yield
With potassium carbonate	91%
Stage #1: 3-hydroxy-4-methylbenzaldehyde With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: methyl iodide In N,N-dimethyl-formamide at 20℃;	91%

: 591-31-1
3-methoxy-benzaldehyde

: 74-88-4
methyl iodide

: 24973-22-6
3-methoxy-4-methylbenzaldehyde

Conditions

Conditions	Yield
Stage #1: 3-methoxy-benzaldehyde With 1-methyl-piperazine; n-butyllithium In tetrahydrofuran; hexane at -20℃; for 0.5h; Stage #2: With sec.-butyllithium In tetrahydrofuran; hexane; cyclohexane for 0.166667h; Stage #3: methyl iodide In tetrahydrofuran; hexane; cyclohexane at -78 - 20℃; Further stages.;	29%
Yield given. Multistep reaction;

: 123-56-8
Succinimide

: 57295-33-7
(2-Bromo-5-methoxy-4-methyl-phenyl)-methanol

A: 57295-32-6
2-Brom-5-methoxy-4-methylbenzaldehyd

B: 24973-22-6
3-methoxy-4-methylbenzaldehyde

C: 90163-04-5
N-(2-Formyl-4-methoxy-5-methylphenyl)succinimid

Conditions

Conditions	Yield
With copper(l) iodide; sodium hydride 1) dimethylacetamide, 2.,5-3 h, r.t., 2) 6 h, reflux; Yield given. Multistep reaction. Yields of byproduct given;
With copper(l) iodide; sodium hydride 1) dimethylacetamide, 2.5-3 h, r.t., 2) 6 h, reflux; Yield given. Multistep reaction. Yields of byproduct given;
With copper(l) iodide; sodium hydride 1) dimethylacetamide, 2.5-3 h, r.t., 2) 6 h, reflux; Yield given. Multistep reaction. Yields of byproduct given;

: 50-00-0
formaldehyd

: 16452-01-0
ortho-cresidine

: 24973-22-6
3-methoxy-4-methylbenzaldehyde

Conditions

Conditions	Yield
(i) aq. NH2OH*HCl, NaOAc, (ii) CuSO4, Na2SO3, aq. NaOAc, (iii) /BRN= 742602/, NaNO2, aq. HCl; Multistep reaction;

: 7151-68-0
3-methoxy-p-toluic acid

: 24973-22-6
3-methoxy-4-methylbenzaldehyde

Conditions

Conditions	Yield
(i) SOCl2, (ii) Li; Multistep reaction;
Multi-step reaction with 2 steps 1: LiAlH4 / tetrahydrofuran / 20 °C 2: MnO2 / CHCl3 / 3 h / Heating View Scheme
Multi-step reaction with 3 steps 1: 91 percent / acetic acid / diethyl ether 2: 88 percent / LiAlH4 / diethyl ether / 2.5 h / Heating 3: 90 percent / active MnO2 / CH2Cl2 / 2 h / Heating View Scheme

: 3-Methoxybenzaldehyde 2,4-Dimethylpent-3-ylimine

: 74-88-4
methyl iodide

A: 56724-03-9
3-methoxy-2-methyl-benzaldehyde

B: 24973-22-6
3-methoxy-4-methylbenzaldehyde

Conditions

Conditions	Yield
With hydrogenchloride; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium 1) ether, cyclohexane, -72 deg C, 1 h; 2) ether, cyclohexane, -72 deg C --> rt; 3) THF, reflux, 2 h; Yield given. Multistep reaction. Yields of byproduct given;

: 586-30-1
3-hydroxy-4-methylbenzoic acid

: 24973-22-6
3-methoxy-4-methylbenzaldehyde

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: K2CO3 / acetone / 10 h / Heating 2: LiAlH4 / tetrahydrofuran / 20 °C 3: MnO2 / CHCl3 / 3 h / Heating View Scheme

: 31680-07-6
4-methyl-3-nitrobenzaldehyde

: 24973-22-6
3-methoxy-4-methylbenzaldehyde

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 2: 91 percent / 33 percent KOH / 45 °C View Scheme

3-Methoxy-4-methylbenzaldehyde Chemical Properties

Product Name: Benzaldehyde,3-methoxy-4-methyl- (CAS NO.24973-22-6)

Molecular Formula: C₉H₁₀O₂
Molecular Weight: 150.17g/mol
Mol File: 24973-22-6.mol
Melting Point: 40.5-41.5
Index of Refraction: 1.542
Molar Refractivity: 44.5 cm³
Molar Volume: 141.3 cm³
Surface Tension 36.1 dyne/cm
Density: 1.062 g/cm³
Flash Point: 105.7 °C
Enthalpy of Vaporization: 48.33 kJ/mol
Boiling Point: 246.2 °C at 760 mmHg
Vapour Pressure: 0.0276 mmHg at 25°C
XLogP3-AA: 2.3
H-Bond Donor: 0
H-Bond Acceptor: 2
Structure Descriptors of Benzaldehyde,3-methoxy-4-methyl- (CAS NO.24973-22-6):
IUPAC Name: 3-methoxy-4-methylbenzaldehyde
Canonical SMILES: CC1=C(C=C(C=C1)C=O)OC
InChI: InChI=1S/C9H10O2/c1-7-3-4-8(6-10)5-9(7)11-2/h3-6H,1-2H3
InChIKey: TVDHPUFLDYYBPO-UHFFFAOYSA-N
Product Categories: FINE Chemical & INTERMEDIATES; Aromatic Aldehydes & Derivatives (substituted); Aldehydes; Phenyls & Phenyl-Het; Benzaldehyde; Adehydes, Acetals & Ketones;Anisoles, Alkyloxy Compounds & Phenylacetates; Phenyls & Phenyl-Het

3-Methoxy-4-methylbenzaldehyde Safety Profile

Safety Information of Benzaldehyde,3-methoxy-4-methyl- (CAS NO.24973-22-6):
Hazard Codes: Xi Irritant
Risk Statements: 36/37/38
R36/37/38:Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36/37/39
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39:Wear suitable protective clothing, gloves and eye/face protection.

3-Methoxy-4-methylbenzaldehyde Specification

Benzaldehyde,3-methoxy-4-methyl- , its CAS NO. is 24973-22-6, the synonym is 3-Methoxy-4-methylbenzaldehyde .

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