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Name |
4,4'-Azobis(4-cyano-1-pentanol) |
EINECS | 1592732-453-0 |
CAS No. | 4693-47-4 | Density | 1.08 g/cm3 |
PSA | 112.76000 | LogP | 1.54816 |
Solubility | N/A | Melting Point |
N/A |
Formula | C12H20N4O2 | Boiling Point | 417.4 °C at 760 mmHg |
Molecular Weight | 252.316 | Flash Point | 206.2 °C |
Transport Information | N/A | Appearance | N/A |
Safety | Risk Codes | N/A | |
Molecular Structure | Hazard Symbols | N/A | |
Synonyms |
Valeronitrile,2,2'-azobis[5-hydroxy-2-methyl- (8CI);2,2'-Azobis(5-hydroxy-2-methylvaleronitrile);4,4'-Azobis(4-cyanopentanol);d,d'-Azobis(d-cyanopentanol); |
Article Data | 2 |
Conditions | Yield |
---|---|
With hydrogenchloride; bromine; hydrazinium sulfate 1.) water, 20 deg C, 72 h, 2.) 4 h, 0 deg C; Yield given. Multistep reaction; |
4,4′-azobis(4-cyano-1-pentanol)
t-Butyldioxycarbonylbutyrylchlorid
Conditions | Yield |
---|---|
With pyridine at -0.1 - 9.9℃; | 98% |
4,4′-azobis(4-cyano-1-pentanol)
3-(t-Butylperoxycarbonyl)-propionyl chloride
Conditions | Yield |
---|---|
With pyridine at -0.1 - 9.9℃; | 96.6% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 2h; | 95% |
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide In water at 30℃; for 4h; | 85% |
4,4′-azobis(4-cyano-1-pentanol)
2-dodecylsulfanylthiocarbonylsulfanyl-2-methyl-propionic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; | 51% |
4,4′-azobis(4-cyano-1-pentanol)
bis(dodecylsulfanyl thiocarbonyl)disulfide
S-dodecyl-S'-[methylhydroxypropylcyanomethyl]trithiocarbonate
Conditions | Yield |
---|---|
In ethyl acetate for 24h; Reflux; | 48% |
bis(thiobenzoyl) disulfide
4,4′-azobis(4-cyano-1-pentanol)
4-cyano-1-hydroxypent-4-yl dithiobenzoate
Conditions | Yield |
---|---|
In ethyl acetate at 70℃; for 24h; | 46% |
In ethyl acetate at 70℃; for 24h; | 46% |
4,4′-azobis(4-cyano-1-pentanol)
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 95 percent / NEt3 / CH2Cl2 / 2 h / 20 °C 2: 64 percent / KH / dimethylsulfoxide; tetrahydrofuran / 1.67 h / 20 °C View Scheme |
Molecular Structure of 4,4'-Azobis(4-cyano-1-pentanol) (CAS No.4693-47-4):
Molecular Formula: C12H20N4O2
Molecular Weight: 252.31
CAS No: 4693-47-4
IUPAC Name: 2-[(2-Cyano-5-hydroxypentan-2-yl)diazenyl]-5-hydroxy-2-methylpentanenitrile
H bond acceptors: 6
H bond donors: 2
Freely Rotating Bonds: 10
Polar Surface Area: 112.76 Å2
Index of Refraction: 1.515
Molar Refractivity: 70.18 cm3
Molar Volume: 232.3 cm3
Surface Tension: 43.7 dyne/cm
Density: 1.08 g/cm3
Flash Point: 206.2 °C
Enthalpy of Vaporization: 77.48 kJ/mol
Boiling Point: 417.4 °C at 760 mmHg
Vapour Pressure: 1.03E-08 mmHg at 25°C
InChI: InChI=1/C12H20N4O2/c1-11(9-13,5-3-7-17)15-16-12(2,10-14)6-4-8-18/h17-18H,3-8H2,1-2H3
InChIKey: IWTIJBANDVIHPX-UHFFFAOYAM
Std. InChI: InChI=1S/C12H20N4O2/c1-11(9-13,5-3-7-17)15-16-12(2,10-14)6-4-8-18/h17-18H,3-8H2,1-2H3
Std. InChIKey: IWTIJBANDVIHPX-UHFFFAOYSA-N
Product Categories: Industrial/Fine Chemicals;Active Pharmaceutical Ingredients
4,4'-Azobis(4-cyano-1-pentanol) (CAS No.4693-47-4), its synonyms are 2,2'-Diazene-1,2-diylbis(5-hydroxy-2-methylpentanenitrile) ; Pentanenitrile, 2,2'-(1,2-diazenediyl)bis[5-hydroxy-2-methyl- .