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959-23-9

959-23-9

Identification

  • Product Name:2-Propen-1-one,1-(4-methoxyphenyl)-3-phenyl-

  • CAS Number: 959-23-9

  • EINECS:

  • Molecular Weight:238.286

  • Molecular Formula: C16H14 O2

  • HS Code:2914509090

  • Mol File:959-23-9.mol

Synonyms:Chalcone,4'-methoxy- (6CI,7CI,8CI); 1-(4-Methoxyphenyl)-3-phenyl-2-propen-1-one;1-(4-Methoxyphenyl)-3-phenylpropenone;1-(p-Methoxyphenyl)-3-phenyl-2-propen-1-one; 4-Methoxyphenyl styryl ketone;4'-Methoxychalcone; NSC 37157

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Safety information and MSDS view more

  • Pictogram(s):

  • Hazard Codes:Xi

  • Signal Word:Warning

  • Hazard Statement:H315 Causes skin irritationH319 Causes serious eye irritation H335 May cause respiratory irritation

  • First-aid measures: General adviceConsult a physician. Show this safety data sheet to the doctor in attendance.If inhaled If breathed in, move person into fresh air. If not breathing, give artificial respiration. Consult a physician. In case of skin contact Wash off with soap and plenty of water. Consult a physician. In case of eye contact Rinse thoroughly with plenty of water for at least 15 minutes and consult a physician. If swallowed Never give anything by mouth to an unconscious person. Rinse mouth with water. Consult a physician.

  • Fire-fighting measures: Suitable extinguishing media Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide. Wear self-contained breathing apparatus for firefighting if necessary.

  • Accidental release measures: Use personal protective equipment. Avoid dust formation. Avoid breathing vapours, mist or gas. Ensure adequate ventilation. Evacuate personnel to safe areas. Avoid breathing dust. For personal protection see section 8. Prevent further leakage or spillage if safe to do so. Do not let product enter drains. Discharge into the environment must be avoided. Pick up and arrange disposal. Sweep up and shovel. Keep in suitable, closed containers for disposal.

  • Handling and storage: Avoid contact with skin and eyes. Avoid formation of dust and aerosols. Avoid exposure - obtain special instructions before use.Provide appropriate exhaust ventilation at places where dust is formed. For precautions see section 2.2. Store in cool place. Keep container tightly closed in a dry and well-ventilated place.

  • Exposure controls/personal protection:Occupational Exposure limit valuesBiological limit values Handle in accordance with good industrial hygiene and safety practice. Wash hands before breaks and at the end of workday. Eye/face protection Safety glasses with side-shields conforming to EN166. Use equipment for eye protection tested and approved under appropriate government standards such as NIOSH (US) or EN 166(EU). Skin protection Wear impervious clothing. The type of protective equipment must be selected according to the concentration and amount of the dangerous substance at the specific workplace. Handle with gloves. Gloves must be inspected prior to use. Use proper glove removal technique(without touching glove's outer surface) to avoid skin contact with this product. Dispose of contaminated gloves after use in accordance with applicable laws and good laboratory practices. Wash and dry hands. The selected protective gloves have to satisfy the specifications of EU Directive 89/686/EEC and the standard EN 374 derived from it. Respiratory protection Wear dust mask when handling large quantities. Thermal hazards

Supplier and reference price

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  • Manufacture/Brand:TRC
  • Product Description:4''-Methoxychalcone
  • Packaging:25g
  • Price:$ 75
  • Delivery:In stock
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  • Manufacture/Brand:Rieke Metals
  • Product Description:1-(4-methoxyphenyl)-3-phenylprop-2-en-1-one
  • Packaging:5g
  • Price:$ 1728
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  • Manufacture/Brand:Rieke Metals
  • Product Description:1-(4-methoxyphenyl)-3-phenylprop-2-en-1-one
  • Packaging:1g
  • Price:$ 661
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  • Manufacture/Brand:Oakwood
  • Product Description:1-(4-Methoxyphenyl)-3-phenylprop-2-en-1-one 95%
  • Packaging:1g
  • Price:$ 10
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  • Manufacture/Brand:Matrix Scientific
  • Product Description:1-(4-Methoxyphenyl)-3-phenylprop-2-en-1-one 97%
  • Packaging:50g
  • Price:$ 198
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  • Manufacture/Brand:Matrix Scientific
  • Product Description:1-(4-Methoxyphenyl)-3-phenylprop-2-en-1-one 97%
  • Packaging:1g
  • Price:$ 29
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  • Manufacture/Brand:Matrix Scientific
  • Product Description:1-(4-Methoxyphenyl)-3-phenylprop-2-en-1-one 97%
  • Packaging:10g
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  • Manufacture/Brand:Heterocyclics
  • Product Description:4'-Methoxychalcone 97%
  • Packaging:25g
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  • Manufacture/Brand:Heterocyclics
  • Product Description:4'-Methoxychalcone 97%
  • Packaging:100g
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  • Manufacture/Brand:Crysdot
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Relevant articles and documentsAll total 148 Articles be found

New pyrimidine derivatives as efficient organic inhibitors on mild steel corrosion in acidic medium: Electrochemical, SEM, EDX, AFM and DFT studies

Yadav,Kumar,Sinha,Bahadur,Ebenso

, p. 135 - 145 (2015)

New pyrimidine derivatives, namely, 7-methoxypyrido [2,3-d]pyrimidin-4-amine (MPPA) and 4-amino-7-methoxypyrido[2,3-d]pyrimidin-2(1H)-one (AMPO) were synthesized and their inhibitive action against the corrosion of mild steel in 15% HCl solution was studi

Synthesis of lithium/cesium-Zagronas from zagrosian natural asphalt and study of their activity as novel, green, heterogeneous and homogeneous nanocatalysts in the Claisen–Schmidt and Knoevenagel condensations

Soleiman-Beigi, Mohammad,Ghalavand, Saba,Venovel, Hadis Gholami,Kohzadi, Homa

, p. 3267 - 3279 (2021/06/17)

A novel, heterogeneous and homogeneous basic nanocatalysts were synthesized by grafting of lithium and cesium on zagrosian natural asphalt sulfonate (Li/Cs-Zagronas). The activity of these catalysts was examined in the Claisen–Schmidt and Knoevenagel condensations under mild reaction conditions. Li/Cs-Zagronas were characterized by FT-IR spectroscopy, scanning electron microscopy, X-ray diffraction, energy-dispersive spectroscopy, inductively coupled plasma and thermogravimetric analysis techniques. These nanocatalysts were removed by simple filtration and reused several times without any deterioration of activity.

Selective catalytic synthesis of α-alkylated ketones and β-disubstituted ketones via acceptorless dehydrogenative cross-coupling of alcohols

Bhattacharyya, Dipanjan,Sarmah, Bikash Kumar,Nandi, Sekhar,Srivastava, Hemant Kumar,Das, Animesh

supporting information, p. 869 - 875 (2021/02/06)

Herein, a phosphine-free pincer ruthenium(III) catalyzed β-alkylation of secondary alcohols with primary alcohols to α-alkylated ketones and two different secondary alcohols to β-branched ketones are reported. Notably, this transformation is environmentally benign and atom efficient with H2O and H2 gas as the only byproducts. The protocol is extended to gram-scale reaction and for functionalization of complex vitamin E and cholesterol derivatives.

Activated charcoal-mediated synthesis of chalcones catalyzed by NaOH in water

Tanemura, Kiyoshi,Rohand, Taoufik

supporting information, (2021/02/27)

A variety of chalcones were synthesized in good yields by the activated charcoal-mediated aldol reactions between benzaldehydes and acetophenones catalyzed by NaOH in water. 2,6-Bis((E)-benzylidene)cyclohexan-1-ones were prepared by the aldol reactions between benzaldehydes and cyclohexanone. Activated charcoal could be recycled five times without the significant decrease of yields.

Synthesis of chalcone derivatives by phthalhydrazide-functionalized tio2-coated nano-fe3o4 as a new heterogeneous catalyst

Farahi, Mahnaz,Karami, Bahador,Keshavarz, Raziyeh,Nia, Forough Motamedi

, p. 407 - 414 (2021/09/07)

Phthalhydrazide immobilized on TiO2-coated nano Fe3O4 (Fe3O4-P) was synthesized and characterized by FT-IR, XRD, SEM, EDS and VSM analysis. The resulting magnetic nanocatalyst was used as a catalyst for the synthesis of chalcone derivatives which affords the desired products in good to excellent yields. This catalyst can be isolated readily after completion of the reaction by an external magnetite field and reused several times without significant loss of activity.

Iridium and copper supported on silicon dioxide as chemoselective catalysts for dehydrogenation and borrowing hydrogen reactions

Zhu, Guanxin,Duan, Zheng-Chao,Zhu, Haiyan,Qi, Minghui,Wang, Dawei

, (2021/04/02)

High active ligand usually plays an important role during catalysis and synthesis chemistry. A new and efficient benzotriazole-pyridinyl-silane ligand (BPS) was designed, and the corresponding iridium and copper catalysts were synthesized and thoroughly characterized by means of EDS, TEM, and XPS. The resulting iridium composite revealed excellent catalytic activity for the reaction of tert-butanesulfinamide with benzyl alcohols, while copper catalyst could realize the synthesis of unsaturated carbonyl compounds through the reaction of benzyl alcohols with ketones. This provided an efficient method for selective synthesis of unsaturated carbonyl compounds from benzyl alcohols and ketones in high yields with good recovery performance.

Process route upstream and downstream products

Process route

1-(4-methoxyphenyl)ethanone
100-06-1

1-(4-methoxyphenyl)ethanone

benzyl alcohol
100-51-6,185532-71-2

benzyl alcohol

4'-methoxychalcone
959-23-9

4'-methoxychalcone

Conditions
Conditions Yield
With oxygen; caesium carbonate; In acetonitrile; at 20 ℃; for 24h; chemoselective reaction;
84%
With graphite oxide; at 80 ℃; for 24h;
48%
With graphite oxide; at 80 ℃; for 24h;
48%
With chromium(VI) oxide; at 0 - 56 ℃; for 10h;
65 %Chromat.
With ceria; In isopropyl alcohol; at 150 ℃; for 12h; chemoselective reaction;
cinnamoyl chloride
102-92-1,17082-09-6

cinnamoyl chloride

methoxybenzene
100-66-3

methoxybenzene

4'-methoxychalcone
959-23-9

4'-methoxychalcone

Conditions
Conditions Yield
With zinc(II) oxide; at 25 - 30 ℃; for 0.166667h; regioselective reaction;
92%
With copper(II) ferrite; In 1,2-dichloro-ethane; at 80 ℃; for 24h;
70%
With o-tetrachloroquinone; (η5,η5-(C5H4)2SiMe2)Mo2(CO)6; In 1,2-dichloro-ethane; at 80 ℃; for 24h; Reagent/catalyst; Temperature; Inert atmosphere; Schlenk technique;
68.4%
With C18H10ClO3Re; In 1,2-dichloro-ethane; at 84 ℃; for 24h; Reagent/catalyst; Catalytic behavior; Inert atmosphere; Schlenk technique; Green chemistry;
30.4%
With carbon disulfide; aluminium trichloride;
rac-1-(4-methoxyphenyl)-ethanol
3319-15-1

rac-1-(4-methoxyphenyl)-ethanol

benzyl alcohol
100-51-6,185532-71-2

benzyl alcohol

4'-methoxychalcone
959-23-9

4'-methoxychalcone

Conditions
Conditions Yield
With [Ni(dmpymt)2]6; potassium hydroxide; In toluene; tert-butyl alcohol; at 70 ℃; for 36h; chemoselective reaction; Schlenk technique; Inert atmosphere;
91%
With oxygen; lithium hydroxide; In water; tert-butyl alcohol; at 70 ℃;
85%
benzaldehyde
100-52-7

benzaldehyde

4-methoxyphenylacetylen
768-60-5

4-methoxyphenylacetylen

4'-methoxychalcone
959-23-9

4'-methoxychalcone

Conditions
Conditions Yield
With Hβ zeolite; In water; at 100 ℃; for 20h; Sealed tube;
96%
With graphite oxide; at 100 ℃; for 14h;
50%
With graphite oxide; at 100 ℃; for 14h;
50%
4-methoxyphenylacetylen
768-60-5

4-methoxyphenylacetylen

benzyl alcohol
100-51-6,185532-71-2

benzyl alcohol

4'-methoxychalcone
959-23-9

4'-methoxychalcone

Conditions
Conditions Yield
With graphite oxide; at 80 ℃; for 24h;
50%
With graphite oxide; at 80 ℃; for 24h;
50%
1-(4-methoxylphenyl)-2-propen-1-ol
51410-44-7

1-(4-methoxylphenyl)-2-propen-1-ol

2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole
24388-23-6

2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

4'-methoxychalcone
959-23-9

4'-methoxychalcone

Conditions
Conditions Yield
1-(4-methoxylphenyl)-2-propen-1-ol; With oxygen; palladium diacetate; In N,N-dimethyl-formamide; at 90 ℃; for 4h; under 760.051 Torr; Green chemistry;
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole; With 2.9-dimethyl-1,10-phenanthroline; In N,N-dimethyl-formamide; at 90 ℃; for 18h; Green chemistry;
89%
4-methoxy-benzaldehyde
123-11-5

4-methoxy-benzaldehyde

acetophenone
98-86-2

acetophenone

4'-methoxychalcone
959-23-9

4'-methoxychalcone

Conditions
Conditions Yield
With sodium hydroxide; In ethanol; at 5 - 10 ℃;
94%
With sodium hydroxide; In ethanol; water;
With sodium hydroxide; In methanol; at 20 ℃;
acetophenone; With sodium hydroxide; In ethanol; water; at 0 ℃; for 0.166667h;
4-methoxy-benzaldehyde; In ethanol; water;
4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

phenylacetylene
536-74-3

phenylacetylene

4'-methoxychalcone
959-23-9

4'-methoxychalcone

Conditions
Conditions Yield
phenylacetylene; With Schwartz's reagent; In toluene; at 50 ℃; for 1h;
4-methoxy-benzoyl chloride; bis-triphenylphosphine-palladium(II) chloride; In toluene; at 20 ℃; for 3h; Further stages.;
73%
1-(4-methoxylphenyl)-2-propen-1-ol
51410-44-7

1-(4-methoxylphenyl)-2-propen-1-ol

potassium phenyltrifluoborate

potassium phenyltrifluoborate

4'-methoxychalcone
959-23-9

4'-methoxychalcone

Conditions
Conditions Yield
1-(4-methoxylphenyl)-2-propen-1-ol; With oxygen; palladium diacetate; In N,N-dimethyl-formamide; at 90 ℃; for 4h; under 760.051 Torr; Green chemistry;
potassium phenyltrifluoborate; With 2.9-dimethyl-1,10-phenanthroline; In N,N-dimethyl-formamide; at 90 ℃; for 18h; Green chemistry;
84%
1-(4-methoxyphenyl)-3-phenylprop-2-en-1-ol
13677-45-7

1-(4-methoxyphenyl)-3-phenylprop-2-en-1-ol

(1E)-3-(4-methoxyphenyl)-1-phenylpropene
20442-73-3,35856-80-5

(1E)-3-(4-methoxyphenyl)-1-phenylpropene

1-methoxy-4-[(1E)-3-phenylprop-1-en-1-yl]benzene
35856-81-6

1-methoxy-4-[(1E)-3-phenylprop-1-en-1-yl]benzene

4'-methoxychalcone
959-23-9

4'-methoxychalcone

Conditions
Conditions Yield
With bismuth(lll) trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 1h; chemoselective reaction;
100 mg

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