- Purification of Ethanolamine (2-Aminoethanol)
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Decomposes slightly when distd at atmospheric pressure, with the formation of conducting impurities. Fractional distn at about 12mm pressure is satisfactory. After distn, amine (CAS NO. ) was further purified by repeated washing with ether and crystn from EtOH (at low temperature).
After fractional distn in the absence of CO2, it was twice crystd by cooling, followed by distn. It can be dried by azeotropic distn with dry *benzene.
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