Tetrahedron Letters p. 2503 - 2506 (1987)
Update date:2022-07-29
Topics:
Bose, Ajay K.
Mangiaracina, Pietro
Commercially available tris(3,6-dioxaheptyl)amine (TDA-1) is an effective phase transfer catalyst for reactions with sodium-potassium alloy in tetrahydrofuran.Deoxygenation of acetates, dehalogenation, and hydrolysis of tosylates and mesylates proceed in high yield.The use of a deuterated alcohol during deoxygenation reactions leads to site-specific deuteration.
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