THE PREPARATION OF N-CARBOXYANHYDRIDES OF α-AMINO ACIDS USING BIS(TRICHLOROMETHYL)CARBONATE

DOI: 10.1016/S0040-4039(00)82209-1

Source and publish data:

Tetrahedron Letters p. 5859 - 5862 (1988)

Update date:2022-08-03

Topics:

Authors:

Daly, William H.

Poche, Drew

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Article abstract of DOI:10.1016/S0040-4039(00)82209-1

A syntheis of the N-carboxyanhydrides (NCA's) of several α-amino acids using bis(trichloromethyl)carbonate, 1, is reported.The triphosgene is used to supply phosgene in situ in stoichiometric amounts; it is particularly effective for preparing NCA's of amino acids with long, aliphatic side chains.

Full text of DOI:10.1016/S0040-4039(00)82209-1

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