THE PREPARATION AND CRYSTAL STRUCTURES OF PhSi(OH)2 AND PhSi(OMe)OH

DOI: 10.1016/0022-328X(85)87333-2

Source and publish data:

Journal of Organometallic Chemistry p. 177 - 188 (1985)

Update date:2022-07-29

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Authors:

Aiube, Zakariah H.

Buttrus, Nabeel H.

Eaborn, Colin

Hitchcock, Peter B.

Zora, Jalal A.

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Article abstract of DOI:10.1016/0022-328X(85)87333-2

The silanol Tsi(Ph)Si(H)OH (Tsi= (Me3Si)3C) was prepared by hydrolysis of Tsi(Ph)Si(H)I in aqueous dioxane, and then treated with ICI in CCl4 to give Tsi(Ph)Si(I)OH, which in turn was hydrolysed with H2O/Me2SO to give the diol Tsi(Ph)Si(OH)2.Treatment of

Full text of DOI:10.1016/0022-328X(85)87333-2

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