2148
Russ.Chem.Bull., Int.Ed., Vol. 55, No. 12, December, 2006
Shtel´tser et al.
absorption corrections were applied based on equivalent reflecꢀ
tions with the use of the SADABS program.16 For complex 3,
absorption was ignored. The structure of 4 contains a dichloroꢀ
methane solvate molecule. The H atoms were placed in geoꢀ
metrically calculated positions and refined using a riding
model. All calculations were carried out on a PC with the use of
the program packages.17,18
Rybinskaya, Izv. Akad. Nauk, Ser. Khim., 2002, 1610 [Russ.
Chem. Bull., Int. Ed., 2002, 51, 1754].
7. C. S. W. Lau and W. T. Wong, J. Chem. Soc., Dalton Trans.,
1998, 3391.
8. G. Jia, D. W. Meek, and J. C. Gallucci, Organometallics,
1990, 9, 2549.
9. S. Komiya, A. Yamamoto, and S. Ikeda, Bull. Chem. Soс.
Jpn, 1975, 48, 101.
10. L. Xu and Y. Sasaki, J. Organomet. Chem., 1999, 585, 246.
11. G. R. Grooks, B. F. G. Johnson, J. Lewis, I. G. Williams,
and G. Gamlen, J. Chem. Soc., A, 1969, 2761.
12. C. M. Kepert, G. B. Deacon, L. Spiccia, G. D. Fallon,
B. W. Skelton, and A. H. White, J. Chem. Soc., Dalton Trans.,
2000, 2867.
This study was financially supported by the Russian
Foundation for Basic Research (Project No. 04ꢀ03ꢀ
32371).
References
13. E. Rosenberg, S. E. Kabir, K. J. Hardcastle, M. Day, and
E. Wolf, Organometallics, 1990, 9, 2214.
1. M. I. Rybinskaya, L. V. Rybin, S. V. Osintseva, F. M.
Dolgushin, A. I. Yanovskii, and Yu. T. Struchkov, Izv. Akad.
Nauk, Ser. Khim., 1995, 159 [Russ. Chem. Bull., 1995, 44,
154 (Engl. Transl.)].
2. N. A. Shtel´tser, L. V. Rybin, M. I. Rybinskaya, S. V.
Osintseva, P. V. Petrovskii, and F. M. Dolgushin, Izv. Akad.
Nauk, Ser. Khim., 2002, 1624 [Russ. Chem. Bull., Int. Ed.,
2002, 51, 1771].
3. L. V. Rybin and M. I. Rybinskaya, Usp. Khim., 1993, 62, 680
[Russ. Chem. Rev., 1993, 62 (Engl. Transl.)].
4. M. I. Bruce, Comprehensive Organometallic Chemistry,
Eds G. Wilkinson, F. G. A. Stone, and E. W. Abel, Pergamon
Press, Oxford, 1982, 4, 867.
14. S. Aime, G. Jannon, D. Osella, A. J. Arce, and A. J.
Deeming, J. Chem. Soc., Dalton Trans., 1984, 1987.
15. G. Gervasio, D. Marabello, P. J. King, E. Sappa, and
A. Secco, J. Organomet. Chem., 2003, 671, 137.
16. G. M. Sheldrick, SADABS, Bruker/Siemens Area Detector
Absorption Correction Program, v. 2.01, Bruker AXS, Madiꢀ
son (Wisconsin, USA), 1998.
17. SMART V5.051 and SAINT V5.00, Area Detector Control and
Integration Software, Bruker AXS Inc., Madison (WIꢀ53719,
USA), 1998.
18. G. M. Sheldrick, SHELXTLꢀ97, V. 5.10, Bruker AXS Inc.,
Madison (WIꢀ53719, USA), 1997.
5. R. K. Pomeroy, Comprehensive Organometallic Chemistry II,
Eds E. W. Abel, F. G. A. Stone, and G. Wilkinson, Pergamon
Press, Oxford, 1995, 7, 835.
6. S. V. Osintseva, F. M. Dolgushin, P. V. Petrovskii, N. A.
Shtel´tser, A. Z. Kreindlin, L. V. Rybin, and M. I.
Received April 24, 2006;
in revised form September 19, 2006