Tetrahedron Letters p. 2879 - 2880 (1986)
Update date:2022-07-29
Topics:
Ishihara, Takashi
Yamasaki, Yasuhiro
Ando, Teiichi
1-Phosphonyloxy-F-1-alkenephosphonates, easily prepared from F-alkanoic acid chlorides and triethyl phosphite, undergo a unique fluoride ion-catalyzed reaction with primary and secondary amines or alcohols to afford the corresponding α,β-unsaturated F-carboxylic acid derivatives in excellent yields, along with diethyl fluorophosphate and phosphite.
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