Synthesis p. 603 - 606 (1987)
Update date:2022-08-04
Topics:
Tsuji, Jiro
Sugiura, Teruo
Minami, Ichiro
A useful preparative method for 1,2-dienes from 3-methoxycarbonyloxy-1-alkynes by the palladium-catalyzed hydrogenolysis with ammonium formate is described. 3-Methoxycarbonyloxy-1-alkynes are prepared by the addition of magnesium acetylide to ketones or aldehydes, followed by quenching with methyl chloroformate.
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