Tetrahedron Letters p. 5289 - 5292 (1986)
Update date:2022-09-26
Samii, Zakaria K M Abd El
Ashmawy, Mohamed I Al
Mellor, John M
Reaction of manganic acetate with diphenyldisulphide in dichloromethane-trifluoroacetic acid in the presence of allylic esters or amides of allylamine gives trifluoroacetoxysulphides and hence by ready hydrolysis vicinal hydroxysulphides.The regiochemical outcome can be controlled by selection of either an acetyl- or trifluoroacetyl derivative.
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