STEREOSELECTIVE SYNTHESIS OF ERYTHRO- AND THREO-1,2-DIOLS FROM DIKETO SULFIDES VIA CIS-3,4-DIHYDROXYTHIOLANES

DOI: 10.1016/S0040-4039(00)95425-X

Source and publish data:

Tetrahedron Letters p. 1799 - 1802 (1987)

Update date:2022-08-05

Topics:

Authors:

Nakayama, Juzo

Yamaoka, Shoji

Hoshino, Masamatsu

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Article abstract of DOI:10.1016/S0040-4039(00)95425-X

Intramolecular reductive coupling reaction of a series of diketo sulfides (1) by a low-valent titanium reagent at 0 deg C in tetrahydrofuran leads to cis-3,4-dihydroxythiolanes (2) exclusively in 67-89percent yields.Desulfurization of 2 by Raney nickel in

Full text of DOI:10.1016/S0040-4039(00)95425-X

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