ELECTROCHEMICAL HETEROCYCLIZATION OF o-TOLUENESULFONAMIDES TO 3-ALKYL-4,5-DIHYDRO-1,2,4-BENZOTHIADIAZEPINE-1,1-DIOXIDES

DOI: 10.1016/S0040-4020(01)85933-0

Source and publish data:

Tetrahedron p. 1545 - 1552 (1988)

Update date:2022-08-05

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Authors:

Palmisano, Giovanni

Danieli, Bruno

Lesma, Giordano

Fiori, Giorgio

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Article abstract of DOI:10.1016/S0040-4020(01)85933-0

Controlled potential oxidation of a variety of substituted o-toluenesulfonamides at a Pt anode in MeCN using a divided cell provides 3-methyl-4,5-dihydro-1,2,4-benzothiadiazepine-1,1-dioxides selectively and in generally good yields.The scope and limitations of this one-step heterocyclization sequence are also discussed.

Full text of DOI:10.1016/S0040-4020(01)85933-0

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