Tetrahedron p. 4755 - 4764 (1994)
Update date:2022-07-29
Topics: Synthesis Oxidation IR spectroscopy Enantiomer Regioselectivity NMR spectroscopy Reduction Chromatography Recrystallization Mass spectrometry (MS) Protecting group Retrosynthetic analysis Stereoselectivity Catalysis Chirality Functional Group Interconversion Natural product Reaction yield Terpenoid Solvent extraction
Minnaard, Adriaan J.
Wijnberg, Joannes B. P. A.
Groot, Aede de
Starting from the readily available (-)-guaiol the germacrane sesquiterpene (+)-hedycaryol can be synthesized in a 7 steps reaction sequence in an overall yield of 16percent.Additionally, (+)-γ-eudesmol has been synthesized, also starting from (-)-guaiol. - Key Words: sesquiterpenes, germacrane, eudesmane, cadinane, γ-eudesmol.
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