Journal of Organic Chemistry p. 1940 - 1943 (1989)
Update date:2022-08-04
Topics:
Jones, David S.
Srinivasan, Ananthachari
Kasina, Sudhakar
Fritzberg, Alan R.
Wilkening, David W.
Various 3-substituted-1,2-diaminopropane compounds in which the amino groups are protected as bis(carbamates) or bis(sulfonamides) were prepared from the corresponding N,N'-bis-protected 2-(aminomethyl)aziridine derivatives by nucleophilic opening of the aziridine ring.The aziridine derivatives are ultimately derived from readily available 2-hydroxy-1,3-diaminopropane.A variety of nucleophiles can be added to incorporate various functionality (CN, O2CCH3, OH, Cl, CH3, CH2CO2H) in the 3-position of the resulting 1,2-diaminopropane derivatives.
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