Synthesis p. 725 - 727 (1988)
Update date:2022-08-04
Topics:
Datta, A.
Bhattacharjee S.
Ila, H.
Junjappa, H.
Synthesis of novel 2,5-substituted 3-bis(methylthio)methylenetetrahydrofurans 4 by oxymercuration-reduction of α-bis(methylthio)methylene-γ,δ-unsaturated alcohols 2 is reported.The carbinols 2 are obtained from the corresponding allyl-(or 2-methyl-2-propenyl)acylketene dithioacetals 1 by sodium borohydride reduction or by treatment with methylmagnesium iodide.
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