Synthesis of 9-β-D-(Xylofuranosyl)adenine from Adenosine

DOI: 10.1055/s-1989-27258

Source and publish data:

Synthesis p. 383 - 384 (1989)

Update date:2022-09-26

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Authors:

Xi, Cheng

Jun-Dong, Zhang

Li-He, Zhang

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Article abstract of DOI:10.1055/s-1989-27258

Protected adenosine 3 was oxidized using Moffatt reagent to give the 3'-ketoadenosine 4 in 60percent yield.Stereospecific reduction of 4 with sodium borohydride in the presence of triethylamine at -18 deg C followed by deprotection effects the inversion o

Full text of DOI:10.1055/s-1989-27258

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