STUDIES IN MARINE CEMBRANOLIDE SYNTHESIS: A SYNTHESIS OF 2,3,5-TRISUBSTITUTED FURAN INTERMEDIATES FOR LOPHOTOXIN AND PUKALIDE

DOI: 10.1016/S0040-4020(01)81102-9

Source and publish data:

Tetrahedron p. 5283 - 5292 (1989)

Update date:2022-07-31

Topics:

Authors:

Paterson, Ian

Gardner, Mark

Banks, Bernard J.

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Article abstract of DOI:10.1016/S0040-4020(01)81102-9

Pd(0)-catalysed coupling between various furyl zinc or tin compounds and vinyl iodides is demonstrated to be a versatile method for the synthesis of 2,3-dialkyl-5-alkenylfurans like 3, as a potential precursors of the ring system of lophotoxin and pukalide.A possible cyclisation substrate was succesfully prepared by glycol cleavage, 21 --> 24, when alcohol oxidation failed.

Full text of DOI:10.1016/S0040-4020(01)81102-9

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