Sterically Hindered Organometallics. Synthesis of Four-membered Rings containing Tin, Oxygen, and Sulphur. The Crystal Structure of 2,2,4,4-Tetra(2,4,6-tri-isopropylphenyl)-1-oxa-3-thia-2,4-distannetane

DOI: 10.1039/c39890001621

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Journal of the Chemical Society. Chemical communications p. 1621 - 1622 (1989)

Update date:2022-07-29

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Authors:

Brown, Paul

Mahon, Mary F.

Molloy, Kieran C.

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Article abstract of DOI:10.1039/c39890001621

Reaction of Na2S*9H2O with 1,1,2,2-tetra(2,4,6-tri-isopropylphenyl)-1,2-dibromoditin in air yields the sterically hindered four-membered 1-oxa-3-thia-2,4-distannetane ring, which is a distorted rhombohedron containing distinct Sn-S <243.9(4), 243.5(4) pm>

Full text of DOI:10.1039/c39890001621

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