Journal of Organic Chemistry p. 3429 - 3431 (1990)
Update date:2022-08-05
Topics:
Alvarez, Eleuterio
Nunez, Maria Teresa
Martin, Victor S.
A mild procedure to obtain halo diols by opening epoxy alcohols with halogen is described.The method is based on the use of Ti(O-i-Pr)4 and the suitable halogen over allylic and homoallylic epoxy alcohols, affording high regioselectivities and yields.Reaction with enantiomerically enriched epoxides leads selectively to chiral halohydrins.
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