Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry p. 150 - 154 (2011)
Update date:2022-09-26
Topics:
Baranwal, Balram P.
Singh, Alok K.
Varma, Anand
Pandey, Avinash C.
A convenient method to synthesize shape controlled nano-sized metal-organic frameworks (MOFs) has been explored to prepare some novel mixed-ligand complexes of titanium(IV) with the general formula [Ti(acac)Cl 2-n(OOCC15H31)(SB)n] (where Hacac = acetylacetone, HSB = Schiff bases and n = 1 or 2). They have been synthesized by stepwise substitutions of chloride ions from titanium(IV) chloride. The complexes were characterized by elemental analyses, molecular weight determinations, spectral, and TEM studies. Coordination number 7 and 8 was assigned for titanium(IV) in the complexes. The powder XRD, TEM, and SAED studies indicates that these complexes are nano-sized having poor crystalline nature. Taylor & Francis Group, LLC.
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Doi:10.1016/j.tet.2011.01.023
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