Journal of the Chemical Society, Dalton Transactions p. 981 - 984 (1993)
Update date:2022-08-06
Topics:
Blake, Alexander J.
Dyson, Paul J.
Johnson, Brian F. G.
Martin, Caroline M.
Nairn, Jacqueline G. M.
et al.
A new, more convenient route to the benzene cluster a key intermediate compound a = 8.932(8), b = 17.387(13), c = 14.833(15) Angstroem, β = 105.69(6) deg and Z = 4.The three osmium atoms form a regular triangle with a mean Os-Os distance of 2.877(12) Angstroem.Two osmium atoms, Os(1) and Os(2), are co-ordinated to four carbonyl ligands and one, Os(3), co-ordinates to two carbonyl ligands.All carbonyl ligands are terminal and approximately linear.The cyclohexadiene ligand is η4 co-ordinated to Os(3) via the 1,3-diene moiety, donating four electrons in total.On thermolysis, this compound is converted to
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