Journal of Crystallographic and Spectroscopic Research p. 139 - 144 (1990)
Update date:2022-08-02
Topics:
Malawska, B.
Gorczyca, M.
Wieczorek, W.
The N-(2-phenylethyl)amide of α-(1',1'-ethylenedioxy)-ethyl-γ-hydroxybutyric acid (II) and the N-(p-methoxybenzyl)amide of α-(1',1'-ethylenedioxy)-ethyl-γ-hydroxybutyric acid (III) have been synthesized and the crystal structure of III has been solved.Compound III, C16H23O5N, crystallizes in the monoclinic space group P21/c with a = 12.572(2), b = 11.149(2), c = 12.317(2) Angstroem and β = 106.53(1) deg.The structure was solved by direct methods, and refined by full-matrix least squares to give R = 0.040 (Rw = 0.047) for 2004 intensities.The dioxolane ringhas a deformed half-chair conformation.
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