Advanced Synthesis and Catalysis p. 55 - 58 (2006)
Update date:2022-08-03
Topics:
Ahn, Jeong-Ae
Chang, Duck-Ho
Young, Jun Park
Ye, Rim Yon
Loupy, Andre
Jun, Chul-Ho
A highly efficient C-C bond cleavage of unstrained aliphatic ketones bearing β-hydrogens with olefins was achieved using a chelation-assisted catalytic system consisting of (Ph3P)3RhCl and 2-amino-3-picoline by microwave irradiation under solvent-free conditions. The addition of cyclohexylamine catalyst accelerated the reaction rate dramatically under microwave irradiation compared with the classical heating method.
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