Palladium(II)-Catalyzed Diastereoselective Acetalization of Hydroxyalkenes

DOI: 10.1246/cl.1990.1387

Source and publish data:

Chemistry Letters p. 1387 - 1390 (1990)

Update date:2022-08-03

Topics:

Authors:

Hosokawa, Takahiro

Nakajima, Fumio

Iwasa, Shooji

Murahashi, Shun-Ichi

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Article abstract of DOI:10.1246/cl.1990.1387

Pd(II)-Catalyzed cyclization of methyl (2S,3S)-2-allyl-3-hydroxybutyrate with methanol gives (2R,4S,5S)-2,5-dimethyl-2-methoxy-4-methoxycarbonyltetrahydrofuran in 88percent de.The cyclization of (2R,3S)-2-allyl-1,3-butandiol gives homochiral bicyclic acetal 3 (R¹ = Me).

Full text of DOI:10.1246/cl.1990.1387

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