Synlett p. 1174 - 1178 (2011)
Update date:2022-08-04
Topics:
Chen, Guo-Qiang
Xu, Zhen-Jiang
Liu, Yungen
Zhou, Cong-Ying
Che, Chi-Ming
A facile method for the construction of amide compounds from aldehydes by an iron-catalyzed nitrene insertion reaction has been developed. Both aryl and aliphatic aldehydes can directly afford the corresponding amides with an iron(II)-terpyridine (tpy) complex formed in situ as catalyst, and PhI=NTs as nitrogen source under mild reaction conditions. An ESI-MS study revealed the formation of [Fe(tpy)NTs)]+ as a reaction intermediate. Georg Thieme Verlag Stuttgart - New York.
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