Tetrahedron Letters p. 5609 - 5612 (1990)
Update date:2022-08-03
Topics:
Krishnan
Sampson
A 5-step synthesis of terminally unsaturated β-fluoro-α,β-unsaturated esters and nitriles 1 is described. Substantial amounts of a deoxygenative side reaction were observed during the key fluoro-Pummerer rearrangement step in the routes leading to the nitriles 1c and 1d.
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Doi:10.1016/S0040-4039(00)98033-X
(1990)Doi:10.1016/S0040-4020(01)90063-8
(1990)Doi:10.1002/anie.201008212
(2011)Doi:10.1021/jo201191x
(2011)Doi:10.1016/j.bmcl.2011.06.009
(2011)Doi:10.1039/P19900003113
(1990)
