Journal of the Chemical Society. Chemical communications p. 43 - 44 (1991)
Update date:2022-08-05
Topics:
Sakakibara, Akihito
Kabe, Yoshio
Shimizu, Toshio
Ando, Wataru
Photochemical reaction of hexamesitylcyclotrisilane 1 or tetramesityldisilene 2 with azobenzene produces silanol 5 via hydrolysis of diazasilacyclopropane 3 and/or 1,2-diaza-3,4-disilacyclobutane 4; the structure of 4 has been confirmed by variable temperature 1H NMR spectroscopy and single-crystal X-ray diffraction, the existence of an Si2N2 ring system is demonstrated.
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(1991)
