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Basic Information
CAS No.: 1010396-29-8
Name: S-23
Article Data: 3
Molecular Structure:
Molecular Structure of 1010396-29-8 (S-23)
Formula: C18H13ClF4N2O3
Molecular Weight: 416.759
Synonyms: S-23;(S)-3-(4-Chloro-3-fluorophenoxy)-N-(4-cyano-3-trifluoromethylphenyl)-2-hydroxy-2-methylpropionamide;(2S)-3-(4-Chloro-3-fluorophenoxy)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methylpropanamide;S 23 (contraceptive)
EINECS: -0
Density: 1.48±0.1 g/cm3(Predicted)
Melting Point: 119-121 °C
Boiling Point: 577.1±50.0 °C(Predicted)
Hazard Symbols: 19161994
Risk Codes: 19161994
PSA: 82.35000
LogP: 4.21108
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Synthetic route
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

Conditions
ConditionsYield
Stage #1: (2R)-3-bromo-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methylpropanamide With potassium carbonate for 2h; Reflux;
Stage #2: 4-chloro-3-fluorophenol With potassium carbonate In isopropyl alcohol for 3h; Reflux;		70.5%
With potassium carbonate In isopropyl alcohol for 3h; Reflux;70.5%
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

Conditions
ConditionsYield
With potassium carbonate In butanone Reflux;
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4-amino-2-trifluoromethylbenzonitrile

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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: thionyl chloride / tetrahydrofuran / 3 h / 4 °C / Inert atmosphere
1.2: 20 °C
2.1: potassium carbonate / isopropyl alcohol / 3 h / Reflux
View Scheme
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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N,N-Dimethylcarbamoyl chloride

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Conditions
ConditionsYield
Stage #1: (S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃;
Stage #2: N,N-Dimethylcarbamoyl chloride In N,N-dimethyl-formamide; mineral oil at 20℃;		155 g
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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methanesulfonyl chloride

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Conditions
ConditionsYield
Stage #1: (S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide With sodium hydride In tetrahydrofuran; mineral oil at 0℃;
Stage #2: methanesulfonyl chloride In tetrahydrofuran; mineral oil at 20℃;
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n-hexanoic anhydride

1010396-29-8

(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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Conditions
ConditionsYield
In pyridine Reflux;70 g
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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acetic anhydride

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In pyridine Reflux;0.4 g
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nicotinic anhydride

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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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Conditions
ConditionsYield
In pyridine for 10h; Reflux;100 g
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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benzoic acid anhydride

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Conditions
ConditionsYield
In pyridine117 g
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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-1320721613-17791785910

    Address:No.53 Da Qing Lu

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  • S-23

  • Casno:

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    S-23

    Min.Order: 0

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    Capacity: We have our own factory in China with 50,0000mt. yearly capacity.Certificate:We have done ISO, Kosher, Reach to serve our customers better, you can trust our quality.Experience:We have done export for 15 years,we have good reputation in gl

    GIHI CHEMICALS CO.,LIMITED, its former company is a small manufacturer who is specialized in the production of ester products which are used in the daily chemicals ,cosmetic produc

  •  GIHI CHEMICALS CO.,LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86217390

    Address:No.567 Dengcai Street,Sandun,Westlake District,Hangzhou310030,Zhejiang,China.

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  • S-23

  • Casno:

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    S-23

    Min.Order: 0

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    best seller Application:API

    Xi'an Changyue Biotechnology Co., Ltd. was established in October 2003 and is located in Xi'an High-tech Industrial Development Park. It is a company specializing in the extraction

  •  Xian Changyue Biological Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:+86-029-62886900

    Address:Keji Road NO.70

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  • S-23

  • Casno:

    1010396-29-8

    S-23

    Min.Order: 0

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    1,we produce and sell good chemicals around the world.2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%.3,our staff consists of highly qualified in

    Wuhan Circle Star Bio-medic Technology co.,Ltd is located in wuhan, the central city of China, the core of the Changjiang river economic belt and known as the "thoroughfare of nin

  •  Wuhan Circle Star Chem-medical Technology co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-13437180835

    Address:Experimental Building 311-15, Nuclear Magnetic Spectrometer Industry Base, No. 128 Guanggu 7th Road, Donghu New Technology Development Zone, Wuhan (Wuhan Area, Free Trade Zone)

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  • S-23

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    S-23

    Min.Order: 1 Gram

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    BOC Sciences provides a wide range of research chemicals and biochemicals including inhibitors, building blocks, GMP Products, impurities and metabolites, APIs for Veterinary, Natural Compounds, ADCs, Stem Cell Molecule and chiral compounds. https:

    BOC Sciences is a brand of BOCSCI Inc. We leverage our wide spectrum of business in the fields of development, manufacturing, marketing, and distribution to help you make best-info

  •  BOC Sciences

    United States  |  Contact Details

    Business Type:Trading Company

    Tel:1-631-485-4226

    Address:Ramsey Road

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  • S-23

  • Casno:

    1010396-29-8

    S-23

    Min.Order: 0

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    factory?direct?sale Application:healing drugs

    Antimex Chemical Limied, was founded in 2001, we are specializing in manufacturing & researching of Active pharmaceutical Ingredients,Veterinary pharm APIs,cosmetic ingredients,and

  •  Antimex Chemical Limied

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-21-50563169

    Address:Room1027,No.Jinyu Road,Pudong

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  • S 23 CAS No.1010396-29-8

  • Casno:

    1010396-29-8

    S 23 CAS No.1010396-29-8

    Min.Order: 0

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    Factory supply high purity low priceAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China

    Guangdong Juda Chemical Industrial Co.,Limited is a company specializing in APIs,pharmaceutical intermediates, electronic chemicals, plant extracts,fine chemicals and cosmetics raw

  •  Guangdong Juda Chemical Industrial Co.,Limited

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86 13510152023(whatsapp)

    Address:Guangzhou chemical city Tianhe District Guangzhou Guangdong China

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  • S-23

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    1010396-29-8

    S-23

    Min.Order: 0

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    best seller Application:API

    DB Biotech co., ltd is a global and professional supplier for plant extracts and functional ingredients, the company is based in XI’an city, which is famous city for the producttio

  •  DB BIOTECH CO., LTD

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86--1829 2989 553

    Address:No.99 Road, Xi'an, China

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  • S-23

  • Casno:

    1010396-29-8

    S-23

    Min.Order: 0

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    Having our own R&D technology team Application:Pharmaceutical field

    Founded in 2008, East Chemsources Limited is a professional manufacturer of supplier in food and beverage, pharmaceuticals, cosmetics and other industries. pharmaceutical field in

  •  EAST CHEMSOURCES LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:15053231572

    Address:No.1581-12,Jinshui Road, Licang, Qingdao,China

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  • S-23 Sarms

  • Casno:

    1010396-29-8

    S-23 Sarms

    Min.Order: 0

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    factory?direct?saleAppearance:powder Storage:In cool ,dry place Package:G/bottle; Kg/bag; 44kg/barrel Application:for pharma use Transportation:Air or sea freight Port:Any main ports of China

    Shaanxi Cuikang Pharmaceutical Technology Co., Ltd. was established in January 2023 and is a wholly-owned subsidiary of Shaanxi Cuicheng Biopharmaceutical Technology Co., Ltd. It i

  •  Shaanxi Cuicheng Biomedical Technology Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+8613119157289

    Address:Chang'an District Western Life Science and Technology Park

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