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Basic Information
CAS No.: 1010396-29-8
Name: S-23
Article Data: 3
Molecular Structure:
Molecular Structure of 1010396-29-8 (S-23)
Formula: C18H13ClF4N2O3
Molecular Weight: 416.759
Synonyms: S-23;(S)-3-(4-Chloro-3-fluorophenoxy)-N-(4-cyano-3-trifluoromethylphenyl)-2-hydroxy-2-methylpropionamide;(2S)-3-(4-Chloro-3-fluorophenoxy)-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methylpropanamide;S 23 (contraceptive)
EINECS: -0
Density: 1.48±0.1 g/cm3(Predicted)
Melting Point: 119-121 °C
Boiling Point: 577.1±50.0 °C(Predicted)
Hazard Symbols: 19161994
Risk Codes: 19161994
PSA: 82.35000
LogP: 4.21108
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

Conditions
ConditionsYield
Stage #1: (2R)-3-bromo-N-[4-cyano-3-(trifluoromethyl)phenyl]-2-hydroxy-2-methylpropanamide With potassium carbonate for 2h; Reflux;
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With potassium carbonate In isopropyl alcohol for 3h; Reflux;70.5%
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

Conditions
ConditionsYield
With potassium carbonate In butanone Reflux;
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4-amino-2-trifluoromethylbenzonitrile

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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: thionyl chloride / tetrahydrofuran / 3 h / 4 °C / Inert atmosphere
1.2: 20 °C
2.1: potassium carbonate / isopropyl alcohol / 3 h / Reflux
View Scheme
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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N,N-Dimethylcarbamoyl chloride

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Conditions
ConditionsYield
Stage #1: (S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃;
Stage #2: N,N-Dimethylcarbamoyl chloride In N,N-dimethyl-formamide; mineral oil at 20℃;		155 g
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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methanesulfonyl chloride

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Conditions
ConditionsYield
Stage #1: (S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide With sodium hydride In tetrahydrofuran; mineral oil at 0℃;
Stage #2: methanesulfonyl chloride In tetrahydrofuran; mineral oil at 20℃;
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n-hexanoic anhydride

1010396-29-8

(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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Conditions
ConditionsYield
In pyridine Reflux;70 g
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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acetic anhydride

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In pyridine Reflux;0.4 g
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nicotinic anhydride

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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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Conditions
ConditionsYield
In pyridine for 10h; Reflux;100 g
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(S)-3-(4-chloro-3-fluorophenoxy)-N-(4-cyano-3-(trifluoromethyl)phenyl)-2-hydroxy-2-methylpropanamide

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benzoic acid anhydride

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Conditions
ConditionsYield
In pyridine117 g
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    Business Type:Trading Company

    Tel:+86-1320721613-17791785910

    Address:No.53 Da Qing Lu

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  • S-23

  • Casno:

    1010396-29-8

    S-23

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Capacity: We have our own factory in China with 50,0000mt. yearly capacity.Certificate:We have done ISO, Kosher, Reach to serve our customers better, you can trust our quality.Experience:We have done export for 15 years,we have good reputation in gl

    GIHI CHEMICALS CO.,LIMITED, its former company is a small manufacturer who is specialized in the production of ester products which are used in the daily chemicals ,cosmetic produc

  •  GIHI CHEMICALS CO.,LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-86217390

    Address:No.567 Dengcai Street,Sandun,Westlake District,Hangzhou310030,Zhejiang,China.

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  • S-23 Sarms

  • Casno:

    1010396-29-8

    S-23 Sarms

    Min.Order: 0

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    High purityAppearance:Flash black powder Storage:Protect from light and keep dry Application:Pharmaceutical intermediates

    Orchid Chemical was established in 2009; we are headquartered in Hangzhou, which is 200 km from China's biggest sea port, Shanghai. Orchid chemical is a joint-venture company, com

  •  ORCHID CHEMICAL SUPPLIES LTD

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86-571-85395792

    Address:607, North Zhongshan Road, Hangzhou 310000 China

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  • S-23

  • Casno:

    1010396-29-8

    S-23

    Min.Order: 0

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    best seller Application:API

    Xi'an Changyue Biotechnology Co., Ltd. was established in October 2003 and is located in Xi'an High-tech Industrial Development Park. It is a company specializing in the extraction

  •  Xian Changyue Biological Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:+86-029-62886900

    Address:Keji Road NO.70

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  • S-23

  • Casno:

    1010396-29-8

    S-23

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    1.best quality in your requirement 2.competitive price in china market 3.mature technical support 4.professional logistic supportAppearance:white powder Storage:Store in dry, dark and ventilated place Package:as per customers'demand Application:Wide

    Jilin Tianyun New Materials Co., Ltd. is a professional production enterprise that production, processing, and export, mainly engaged in various organic chemicals. The company has

  •  Jilin Tianyun New Materials Co., Ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-1863412-4001

    Address:Nanguan District

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  • S-23

  • Casno:

    1010396-29-8

    S-23

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    1,we produce and sell good chemicals around the world.2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%.3,our staff consists of highly qualified in

    Wuhan Circle Star Bio-medic Technology co.,Ltd is located in wuhan, the central city of China, the core of the Changjiang river economic belt and known as the "thoroughfare of nin

  •  Wuhan Circle Star Chem-medical Technology co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-13437180835

    Address:Experimental Building 311-15, Nuclear Magnetic Spectrometer Industry Base, No. 128 Guanggu 7th Road, Donghu New Technology Development Zone, Wuhan (Wuhan Area, Free Trade Zone)

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  • S-23

  • Casno:

    1010396-29-8

    S-23

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    factory?direct?sale Application:healing drugs

    Antimex Chemical Limied, was founded in 2001, we are specializing in manufacturing & researching of Active pharmaceutical Ingredients,Veterinary pharm APIs,cosmetic ingredients,and

  •  Antimex Chemical Limied

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:0086-21-50563169

    Address:Room1027,No.Jinyu Road,Pudong

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  • S-23

  • Casno:

    1010396-29-8

    S-23

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Having our own R&D technology team Application:Pharmaceutical field

    Zhonghe Fountain is striving for R&D,production and distribution cosmetic active ingredients for personal care industry. Zhonghe Fountain always maintains a keen insight into indu

  •  Zhonghe Fountain(Tianjin)Biotech Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-22-28588176

    Address:Tianjin,China

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