Synthesis of bergenin-type C-glucosylarenes

DOI: 10.1016/0008-6215(91)80148-G

Source and publish data:

Carbohydrate Research p. 101 - 107 (1991)

Update date:2022-08-04

Topics: Synthesis NMR spectroscopy Organic synthesis Methylation HPLC Analysis Arene Phenolic C-glycosylation

Authors:

Frick, Wendelin

Schmidt, Richard R.

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Article abstract of DOI:10.1016/0008-6215(91)80148-G

Reaction of 1,2,3-trimethoxybenzene with 2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl trifluoroacetate (5) in the presence of BF3*OEt2 afforded the 4-β-C-glycosylarene 6.Hydrogenolysis of 6, then O-methoxycarbonylation, and bromination gave 1-bromo-2,3,4-tri

Full text of DOI:10.1016/0008-6215(91)80148-G

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Product name:2,3,4-Trimethoxy-6-methoxycarbonyl-1-phenylsulfinyl-5-(2,3,4,6-tetra-O-methoxycarbonyl-β-D-glucopyranosyl)benzene

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