Synthetic Communications p. 653 - 656 (1991)
Update date:2022-09-26
Topics:
Nijs
Verkruijsse
Harder
Van der Kerk
Brandsma
Addition of the allenic amine H2C = C = CHNMe2 and the corresponding N-morpholinoallene to a solution of an aromatic or heteroaromatic aldehyde, RCH = O, and lithium bromide in tetrahydrofuran followed by treatment of the reaction mixture with a small amount of acetic acid at elevated temperatures affords the aldehydes RCH = C (CH2NR'2) CH = O (NR'2 = NMe2 or morpholino) in reasonable yields.
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