Journal of Fluorine Chemistry p. 307 - 316 (1991)
Update date:2022-08-03
Topics:
Pews, R. G.
Gall, J. A.
The preparation of 2,6-difluoroaniline from 1,3,5-trichlorobenzene is described. 1-Chloro-3,5-difluorobenzene prepared via KF exchange on 1,3,5-trichlorobenzene is dichlorinated and nitrated in a single reactor to a mixture of trichlorodifluoronitrobenzenes.The latter are reduced to ca. 4:1 mixture of 2,6-difluoroaniline and 2,4-difluoroaniline.
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Doi:10.1002/chir.22003
(2012)Doi:10.1016/j.carres.2012.01.020
(2012)Doi:10.1021/om00037a039
(1992)Doi:10.1039/c39910000877
(1991)Doi:10.1134/S1070428012020236
(2012)Doi:10.1055/s-1991-26542
(1991)
