Organometallics p. 4031 - 4035 (1991)
Update date:2022-08-03
Topics:
Kreutzer, Kristina A.
Fisher, Richard A.
Davis, William M.
Spaltenstein, Esther
Buchwald, Stephen L.
The trimethylphosphine adducts of zirconocene and hafhocene silyl hydride complexes have been prepared and the X-ray crystal structure of the zirconocene complex has been determined. In addition, the mechanism of formation of these complexes and a study of the reactivity of the zirconocene complex are presented. The complex Cp2Zr(H)(SiPh3)(PMe3) (2) crystallizes in the monoclinic space group P21/c with a = 9.336 (2) ?, b = 28.863 (8) ?, c = 11.051 (3) ?, β = 111.11 (2)°, and Z = 4; Rw = 0.048.
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Doi:10.1021/ic202207e
(2012)Doi:10.1002/hlca.201100238
(2012)Doi:10.1080/00397911.2010.521967
(2012)Doi:10.1016/j.jorganchem.2012.01.021
(2012)Doi:10.1016/0040-4039(91)80604-5
(1991)Doi:10.1016/j.ejmech.2012.05.004
(2012)
